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反式-4-甲基环己胺盐酸盐

产品名称 反式-4-甲基环己胺盐酸盐

CAS号33483-65-7

分子式C7H16ClN

分子量149.66

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  • Mass

    MS-IW-0799          
    trans-4-methylcyclohexylamine hydrochloride
    C7H15N HCl          (Mass of molecular ion:    113)
    

       Source Temperature: 110 °C
       Sample Temperature:  90 °C
       Direct, 75 eV
    

          28.0       2.1
          30.0       1.9
          36.0       9.5
          38.0       3.4
          39.0       1.1
          41.0       2.4
          42.0       1.6
          43.0      10.4
          55.0       1.5
          56.0     100.0
          57.0       4.8
          67.0       1.5
          81.0       3.0
          84.0       5.1
          95.0       1.7
          96.0       1.2
         112.0       1.1
         113.0      17.6
         114.0       2.2
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C7 H15 N 0.036 g : 0.5 ml DMSO-d6
    trans-4-methylcyclohexylamine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.27 B 2.865 C 1.953 D 1.677 E 1.35 F 1.25 G 0.928 J 0.855

         Hz     ppm     Int.
    

       3304.75   8.270    392
       1157.07   2.896     69
       1153.11   2.886     46
       1149.29   2.876     78
       1145.32   2.866    143
       1141.36   2.856     80
       1137.54   2.847     49
       1133.58   2.837     76
        785.98   1.967    163
        780.94   1.955    103
        776.06   1.942    178
        677.95   1.697    190
        676.57   1.693    189
        670.78   1.679    105
        664.06   1.662    207
        560.76   1.404     82
        557.10   1.394     80
        547.94   1.372    172
        544.59   1.363    159
        535.58   1.341    171
        532.38   1.333    169
        523.07   1.309    101
        519.56   1.301    104
        514.68   1.288     73
        511.32   1.280     68
        508.12   1.272     74
        504.61   1.263     58
        503.39   1.260     57
        499.88   1.251     47
        496.52   1.243     42
        398.25   0.997     75
        395.05   0.989     81
        384.98   0.964    184
        382.08   0.957    169
        372.77   0.933    149
        370.18   0.927    160
        358.58   0.898    112
        357.51   0.895    113
        345.31   0.865   1000
        338.90   0.848    938
    

in DMSO-d6



KBr disc



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