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MS-IW-0799 trans-4-methylcyclohexylamine hydrochloride C7H15N HCl (Mass of molecular ion: 113)
Source Temperature: 110 °C Sample Temperature: 90 °C Direct, 75 eV
28.0 2.1 30.0 1.9 36.0 9.5 38.0 3.4 39.0 1.1 41.0 2.4 42.0 1.6 43.0 10.4 55.0 1.5 56.0 100.0 57.0 4.8 67.0 1.5 81.0 3.0 84.0 5.1 95.0 1.7 96.0 1.2 112.0 1.1 113.0 17.6 114.0 2.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H15 N 0.036 g : 0.5 ml DMSO-d6 trans-4-methylcyclohexylamine hydrochloride Assign. Shift(ppm)
A 8.27 B 2.865 C 1.953 D 1.677 E 1.35 F 1.25 G 0.928 J 0.855
Hz ppm Int.
3304.75 8.270 392 1157.07 2.896 69 1153.11 2.886 46 1149.29 2.876 78 1145.32 2.866 143 1141.36 2.856 80 1137.54 2.847 49 1133.58 2.837 76 785.98 1.967 163 780.94 1.955 103 776.06 1.942 178 677.95 1.697 190 676.57 1.693 189 670.78 1.679 105 664.06 1.662 207 560.76 1.404 82 557.10 1.394 80 547.94 1.372 172 544.59 1.363 159 535.58 1.341 171 532.38 1.333 169 523.07 1.309 101 519.56 1.301 104 514.68 1.288 73 511.32 1.280 68 508.12 1.272 74 504.61 1.263 58 503.39 1.260 57 499.88 1.251 47 496.52 1.243 42 398.25 0.997 75 395.05 0.989 81 384.98 0.964 184 382.08 0.957 169 372.77 0.933 149 370.18 0.927 160 358.58 0.898 112 357.51 0.895 113 345.31 0.865 1000 338.90 0.848 938
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