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网站主页CAS数据库列表 3319-99-1更多图谱2-(2-噻吩)吡啶(3319-99-1)核磁图(13CNMR)

2-(2-噻吩)吡啶

产品名称 2-(2-噻吩)吡啶

CAS号3319-99-1

分子式C9H7NS

分子量161.22

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  • Mass

    MS-NW-7147          
    2-(2-thienyl)pyridine
    C9H7NS              (Mass of molecular ion:    161)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          26.0       1.3
          27.0       1.5
          28.0       2.1
          37.0       1.2
          38.0       2.2
          39.0       7.1
          45.0       6.9
          50.0       5.1
          51.0       9.2
          52.0       4.6
          57.0       1.3
          58.0       3.8
          58.5       2.5
          61.0       1.1
          62.0       2.2
          63.0       5.3
          64.0       1.5
          67.0       1.4
          69.0       3.9
          74.0       1.7
          75.0       2.1
          76.0       1.7
          77.0       1.3
          78.0       8.4
          79.0       1.2
          80.0       2.1
          80.5       4.2
          81.0       1.3
          82.0       2.1
          83.0       1.1
          89.0       7.6
          90.0       4.8
          91.0       1.3
          93.0       1.0
         104.0       2.2
         108.0       2.9
         109.0       1.5
         116.0       6.1
         117.0      16.6
         118.0       1.6
         121.0       1.1
         122.0       1.7
         128.0       9.6
         129.0       1.5
         133.0       1.6
         134.0       4.6
         135.0       5.7
         159.0       1.1
         160.0      25.1
         161.0     100.0
         162.0      11.7
         163.0       5.2
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H7 N S 0.047 g : 0.5 ml CDCl3
    2-(2-thienyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.559 B 7.65 C 7.64 D 7.565 E 7.382 F 7.12 G 7.098 J(A,F) = 4.6 HZ. J(D,G) = 3.8 HZ. J(D,E) = 1.3 HZ. J(E,G) = 5.1 HZ. J(B,F) = 6.2 HZ. J(C,F) = 2.3 HZ.

         Hz     ppm     Int.
    

       3428.22   8.579     33
       3424.19   8.568    310
       3423.10   8.566    357
       3422.61   8.565    374
       3421.51   8.562    326
       3419.31   8.556    318
       3417.97   8.553    478
       3416.50   8.549    305
       3414.06   8.543     30
       3069.46   7.681     35
       3067.14   7.675    169
       3065.43   7.671    162
       3063.84   7.667     57
       3063.23   7.665     61
       3062.50   7.663     64
       3060.91   7.659     97
       3059.08   7.655    631
       3057.37   7.651    656
       3054.57   7.644    665
       3053.47   7.641    769
       3052.86   7.639    949
       3052.12   7.637    864
       3051.27   7.635   1000
       3046.51   7.623    177
       3045.41   7.621    164
       3044.19   7.618     71
       3042.85   7.614     55
       3041.87   7.612     39
       3041.14   7.610     37
       3026.00   7.572    756
       3024.90   7.569    762
       3022.34   7.563    765
       3021.12   7.560    771
       2953.00   7.389    736
       2951.78   7.386    706
       2949.58   7.381     68
       2947.88   7.377    780
       2946.78   7.374    774
       2854.49   7.143     42
       2851.44   7.135    398
       2849.12   7.130    351
       2847.66   7.126     91
       2846.56   7.123    400
       2845.21   7.120    386
       2843.99   7.117    385
       2842.77   7.114    393
       2840.94   7.109    944
       2840.45   7.108    471
       2837.89   7.101    442
       2837.28   7.100    899
       2835.94   7.097    829
       2832.28   7.087    765
    


  • 1H NMR 89.56 MHz
    C9 H7 N S 0.043 g : 0.5 ml CDCl3
    2-(2-thienyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.55 B 7.67 C 7.62 D 7.57 E 7.371 F 7.11 G 7.10

         Hz     ppm     Int.
    

        769.88   8.597    181
        768.38   8.580    253
        767.06   8.565    198
        765.06   8.543    206
        763.69   8.528    328
        762.25   8.512    191
        687.44   7.676    442
        685.81   7.658    761
        684.75   7.646    470
        682.38   7.620   1000
        681.00   7.604    819
        679.94   7.593    543
        678.75   7.579    560
        676.25   7.551    536
        675.13   7.539    578
        672.88   7.514     69
        663.75   7.412    410
        662.56   7.398    388
        660.31   7.373     79
        658.63   7.355    625
        657.44   7.341    518
        643.19   7.182    273
        639.13   7.137    792
        638.31   7.128    463
        637.19   7.115    124
        635.50   7.096    655
        634.06   7.080    639
        630.38   7.039    450
        629.75   7.032    221
    

in CDCl3



KBr disc



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