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2,6-di(2-thienyl)pyridine

产品名称 2,6-di(2-thienyl)pyridine

CAS号35299-71-9

分子式C13H9NS2

分子量243.35

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  • Mass

    MS-IW-8143          
    2,6-di(2-thienyl)pyridine
    C13H9NS2            (Mass of molecular ion:    243)
    

       Source Temperature: 140 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          39.0       1.3
          45.0       1.7
          63.0       1.3
          69.0       1.3
          89.0       1.8
          99.5       3.6
         105.0       1.0
         108.0       2.7
         116.0       1.0
         121.5       6.2
         122.0       1.2
         133.0       1.0
         134.0       1.5
         154.0       1.0
         159.0       1.0
         160.0       1.8
         171.0       1.0
         197.0       1.2
         198.0       2.7
         199.0       2.2
         209.0       1.9
         210.0       8.7
         211.0       1.6
         217.0       1.0
         241.0       1.6
         242.0      11.5
         243.0     100.0
         244.0      17.0
         245.0      10.0
         246.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H9 N S2 0.006 g : 0.5 ml CDCl3
    2,6-di(2-thienyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.659 B 7.631 C 7.485 D 7.400 E 7.113 J(A,C)=7.8HZ J(B,D)=1.2HZ J(B,E)=3.8HZ J(D,E)=5.1HZ

         Hz     ppm     Int.
    

       3069.95   7.682    235
       3062.50   7.663    312
       3061.65   7.661    327
       3054.20   7.643    405
       3052.12   7.637    654
       3051.03   7.635    661
       3048.46   7.628    671
       3047.36   7.626    650
       2994.63   7.494   1000
       2986.82   7.474    700
       2963.50   7.416     33
       2960.94   7.409    604
       2959.72   7.406    596
       2955.81   7.396    664
       2954.71   7.394    638
       2847.29   7.125    643
       2843.51   7.116    665
       2842.16   7.112    643
       2838.50   7.103    599
    

in CDCl3



liquid film