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MassMS-NW-7104 4-chloro-3-(trifluoromethyl)aniline C7H5ClF3N (Mass of molecular ion: 195)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
28.0 3.8 31.0 1.2 37.0 1.8 38.0 2.1 39.0 2.6 41.0 3.8 44.5 1.1 45.5 1.1 50.0 1.4 51.0 1.1 52.0 3.3 57.0 1.3 61.0 2.3 62.0 3.9 63.0 8.4 64.0 2.5 65.0 1.9 69.0 2.1 70.0 1.1 70.5 1.7 73.0 2.1 74.0 1.5 75.0 2.8 80.0 8.3 81.0 1.5 83.0 2.4 88.0 3.0 89.0 1.8 90.0 3.9 91.0 2.1 97.5 2.7 99.0 5.0 101.0 1.5 110.0 1.1 113.0 5.5 114.0 1.8 120.0 2.9 125.0 1.2 132.0 5.6 133.0 3.7 139.0 1.5 140.0 7.7 141.0 1.0 143.0 1.1 145.0 8.8 147.0 3.6 148.0 17.4 149.0 1.6 150.0 5.7 159.0 1.1 160.0 11.6 161.0 1.1 167.0 1.7 174.0 2.5 175.0 3.9 176.0 13.9 177.0 2.5 178.0 4.5 179.0 1.1 194.0 2.7 195.0 100.0 196.0 9.1 197.0 33.3 198.0 2.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H5 Cl F3 N 0.042 g : 0.5 ml CDCl3 4-chloro-3-(trifluoromethyl)aniline 
Assign. Shift(ppm)
A 7.221 B 6.950 C 6.718 D 3.83
Hz ppm Int.2890.50 7.233 717 2890.14 7.232 732 2886.84 7.224 51 2881.96 7.212 779 2881.59 7.211 791 2779.17 6.955 970 2776.37 6.948 1000 2770.26 6.932 22 2690.92 6.734 493 2690.31 6.732 499 2688.11 6.727 469 2687.50 6.725 461 2682.37 6.712 459 2681.76 6.711 468 2679.57 6.705 429 2678.96 6.704 423 1531.74 3.833 283
in CDCl3
KBr disc
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