图谱信息 供应商 相关产品
网站主页CAS数据库列表 400-70-4更多图谱2,4-二氯-5-硝基三氟甲基苯(400-70-4)核磁图(1HNMR)

2,4-二氯-5-硝基三氟甲基苯

产品名称 2,4-二氯-5-硝基三氟甲基苯

CAS号400-70-4

分子式C7H2Cl2F3NO2

分子量260

展开


  • Mass

    MS-IW-0099          
    2,4-dichloro-alpha,alpha,alpha-trifluoro-5-nitrotoluene
    C7H2Cl2F3NO2        (Mass of molecular ion:    259)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       2.9
          30.0      68.1
          31.0       3.0
          36.0       2.1
          37.0       4.1
          38.0       1.5
          46.0       2.6
          49.0       1.9
          50.0       7.7
          51.0       1.4
          60.0       1.5
          61.0       4.5
          62.0       3.7
          63.0       1.0
          67.0       1.1
          68.0       1.0
          69.0      19.3
          72.0       3.6
          73.0       9.4
          74.0      24.4
          75.0       9.7
          79.0       1.2
          80.0       1.1
          81.0       2.2
          84.0       6.8
          85.0       8.9
          86.0       3.1
          87.0       4.0
          88.0       1.5
          91.0       5.3
          92.0       4.8
          93.0      11.6
          95.0       1.0
          96.0       1.0
          97.0       4.5
          98.0       1.4
          99.0       7.1
         103.0       1.5
         104.0       2.0
         105.0       1.0
         107.0       1.6
         108.0       7.5
         109.0      19.9
         110.0       3.6
         111.0       6.7
         115.0       1.8
         117.0       2.3
         122.0       1.0
         123.0       6.1
         124.0       1.5
         125.0       1.6
         127.0       2.9
         128.0       4.6
         129.0       3.4
         130.0       1.9
         131.0       3.0
         133.0       2.6
         135.0       1.0
         142.0       2.1
         143.0      47.0
         144.0       5.2
         146.0       1.7
         151.0       3.1
         153.0       5.1
         155.0       1.3
         157.0       1.5
         158.0       1.3
         159.0      11.8
         160.0       1.8
         161.0       3.9
         163.0       5.1
         165.0       4.5
         166.0      58.3
         167.0       4.8
         168.0      19.0
         169.0       1.4
         177.0      14.7
         178.0      55.5
         179.0       9.1
         180.0      18.1
         181.0       3.6
         182.0       1.6
         183.0       1.5
         184.0       1.0
         193.0       3.4
         194.0       5.8
         195.0       2.5
         196.0       3.6
         201.0      40.8
         202.0       2.9
         203.0      26.4
         204.0       1.9
         205.0       4.4
         213.0      84.7
         214.0       6.9
         215.0      54.6
         216.0       4.3
         217.0       9.0
         229.0      76.9
         230.0       6.0
         231.0      50.0
         232.0       3.9
         233.0       8.1
         240.0      11.4
         242.0       7.4
         243.0       6.7
         244.0       1.7
         245.0       4.1
         259.0     100.0
         260.0       8.2
         261.0      64.9
         262.0       5.3
         263.0      10.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H2 Cl2 F3 N O2 0.032 g : 0.5 ml CDCl3
    2,4-dichloro-alpha,alpha,alpha-trifluoro-5-nitrotoluene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.285 B 7.779

         Hz     ppm     Int.
    

       3311.28   8.286   1000
       3108.89   7.780    987
    

in CDCl3



KBr disc



nujol mull