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MassMS-NW-1356 (3-(2-aminoethylamino)propyl)dimethoxy(methyl)silane C8H22N2O2Si (Mass of molecular ion: 206)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 3.3 18.0 2.0 27.0 1.0 28.0 5.9 29.0 5.6 30.0 8.4 31.0 11.7 32.0 8.4 41.0 2.1 42.0 2.9 43.0 4.3 44.0 19.6 45.0 5.2 56.0 2.1 58.0 2.1 59.0 7.6 60.0 1.3 61.0 2.7 63.0 1.0 70.0 1.1 73.0 10.1 74.0 2.0 75.0 20.7 76.0 2.1 77.0 1.3 85.0 1.8 87.0 1.0 88.0 1.5 90.0 2.4 91.0 3.3 98.0 1.1 99.0 1.8 100.0 1.1 101.0 1.1 102.0 3.5 104.0 1.3 105.0 27.2 106.0 2.6 107.0 1.1 112.0 1.8 113.0 1.1 114.0 35.1 115.0 4.5 116.0 2.3 121.0 2.8 130.0 2.4 131.0 1.0 132.0 5.8 133.0 1.2 137.0 1.0 141.0 1.3 142.0 2.1 143.0 1.4 144.0 100.0 145.0 12.7 146.0 4.7 147.0 1.1 159.0 2.7 160.0 2.4 176.0 30.0 177.0 4.2 178.0 1.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H22 N2 O2 Si 0.04 ml : 0.5 ml CDCl3 (3-(2-aminoethylamino)propyl)dimethoxy(methyl)silane 
Assign. Shift(ppm)
A 3.512 B 2.90 to 2.52 C 1.56 D 1.24 E 0.64 F 0.117
Hz ppm Int.314.56 3.513 1000 250.88 2.802 38 250.13 2.793 31 246.94 2.758 48 246.19 2.749 56 242.94 2.713 59 242.13 2.704 70 238.94 2.668 32 238.19 2.660 41 234.75 2.622 44 233.50 2.608 32 227.50 2.541 34 111.31 1.243 139 65.13 0.728 28 10.50 0.118 259
in CDCl3
CCl4 solution
liquid film
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