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MassMS-IW-2194 2,2,2-trifluoro-1-(trifluoromethyl)ethyl methacrylate C7H6F6O2 (Mass of molecular ion: 236)
Source Temperature: 230 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.1 26.0 1.3 27.0 1.3 28.0 1.8 29.0 2.9 31.0 1.0 37.0 1.7 38.0 4.7 39.0 41.8 40.0 11.8 41.0 85.9 42.0 5.2 43.0 1.2 45.0 1.3 51.0 3.1 53.0 1.4 55.0 1.4 57.0 1.1 59.0 1.5 68.0 5.1 69.0 100.0 70.0 4.3 72.0 2.9 82.0 1.5 103.0 1.8 113.0 2.0 151.0 2.1 167.0 1.0 169.0 1.0 172.0 3.0 197.0 5.1 217.0 4.1 221.0 4.4 235.0 3.1 236.0 43.3 237.0 3.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H6 F6 O2 0.05 ml : 0.5 ml CDCl3 2,2,2-trifluoro-1-(trifluoromethyl)ethyl methacrylate 
Assign. Shift(ppm)
A 6.337 B 5.849 C 5.83 D 2.019 J(B,F-19)=6.1HZ
Hz ppm Int.2533.81 6.341 316 2532.84 6.338 435 2531.86 6.336 338 2352.05 5.886 92 2349.61 5.880 23 2345.95 5.871 206 2339.84 5.855 273 2333.74 5.840 222 2331.30 5.834 111 2329.83 5.830 276 2328.86 5.828 294 2328.25 5.826 342 2327.27 5.824 324 2325.68 5.820 112 2321.41 5.809 25 808.23 2.023 835 807.25 2.020 907 806.64 2.019 1000 805.66 2.016 827
in CDCl3
liquid film
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