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MassMS-IW-2186 2,2,2-trifluoro-1-(trifluoromethyl)ethyl acrylate C6H4F6O2 (Mass of molecular ion: 222)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
26.0 5.6 27.0 36.4 28.0 1.0 29.0 2.5 51.0 2.6 53.0 1.6 54.0 1.0 55.0 100.0 56.0 4.5 69.0 17.9 82.0 1.2 113.0 1.8 151.0 1.3 158.0 2.9 183.0 5.7 203.0 1.4 222.0 4.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H4 F6 O2 0.05 ml : 0.5 ml CDCl3 2,2,2-trifluoro-1-(trifluoromethyl)ethyl acrylate 
Assign. Shift(ppm)
A 6.642 B 6.241 C 6.101 D 5.864 J(A,B)=17.3HZ J(A,C)=1.0HZ J(B,C)=10.5HZ J(D,F-19)=6.1HZ
Hz ppm Int.2664.43 6.667 725 2663.45 6.665 786 2647.22 6.624 890 2646.24 6.622 946 2508.30 6.277 728 2497.68 6.250 977 2494.63 6.243 34 2494.26 6.242 34 2491.09 6.234 542 2484.01 6.216 31 2480.47 6.207 845 2443.36 6.114 967 2442.26 6.111 1000 2432.74 6.088 686 2431.76 6.085 729 2362.06 5.911 44 2355.96 5.896 230 2349.85 5.880 554 2346.19 5.871 62 2343.75 5.865 720 2340.21 5.856 55 2337.65 5.850 554 2334.35 5.841 33 2331.42 5.834 235 2325.32 5.819 45
in CDCl3
liquid film
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