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MS-IW-0722 (2,5-dichlorophenyl)hydrazine C6H6Cl2N2 (Mass of molecular ion: 176)
Source Temperature: 250 °C Sample Temperature: 160 °C Reservoir, 75 eV
17.0 1.7 18.0 8.8 28.0 5.5 29.0 2.8 31.0 5.5 36.0 1.6 37.0 1.7 38.0 2.1 39.0 1.1 44.0 1.5 44.5 1.0 45.0 2.2 49.0 1.3 50.0 3.8 51.0 3.6 52.0 3.0 61.0 2.3 62.0 3.4 63.0 5.6 64.0 1.4 73.0 5.5 74.0 5.8 75.0 13.0 76.0 3.1 77.0 7.2 78.0 2.6 83.0 1.0 84.0 1.3 85.0 2.1 86.0 1.0 87.0 1.2 88.0 3.5 89.0 2.2 90.0 3.2 97.0 2.5 98.0 1.5 99.0 2.2 105.0 1.0 109.0 3.7 110.0 2.6 111.0 19.4 112.0 4.0 113.0 6.3 114.0 3.0 124.0 15.0 125.0 4.7 126.0 6.3 127.0 2.1 133.0 35.1 134.0 2.4 135.0 22.3 136.0 1.5 137.0 3.6 139.0 1.1 141.0 25.9 142.0 2.0 143.0 8.3 145.0 1.9 146.0 17.9 147.0 3.7 148.0 11.6 149.0 1.8 150.0 2.1 159.0 7.7 160.0 30.1 161.0 22.1 162.0 20.5 163.0 11.8 164.0 4.0 165.0 1.7 174.0 1.1 175.0 2.0 176.0 100.0 177.0 8.5 178.0 63.6 179.0 4.9 180.0 10.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H6 Cl2 N2 0.037 g : 0.5 ml DMSO-d6 (2,5-dichlorophenyl)hydrazine Assign. Shift(ppm)
A 7.198 B 7.180 C 6.86 D 6.605 E 4.3
Hz ppm Int.
2881.23 7.210 909 2877.81 7.201 23 2876.22 7.197 24 2872.92 7.189 1000 2870.85 7.184 719 2868.29 7.178 717 2861.33 7.160 21 2741.46 6.860 429 2645.02 6.619 545 2642.46 6.612 529 2639.65 6.605 28 2636.60 6.598 495 2634.03 6.591 493 1721.07 4.307 149
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