3,4-二氯苯肼盐酸盐

产品名称 3,4-二氯苯肼盐酸盐

CAS号19763-90-7

分子式C6H7Cl3N2

分子量213.49

¹³CNMR

Mass

MS-KW-0850          
(3,4-dichlorophenyl)hydrazine hydrochloride
C6H6Cl2N2 HCl       (Mass of molecular ion:    176)

   Source Temperature: 160 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      17.0       2.5
      18.0       8.0
      28.0       5.2
      29.0       6.6
      30.0       1.6
      31.0       4.0
      35.0       6.0
      36.0      54.2
      37.0       4.6
      38.0      19.5
      39.0       2.0
      44.5       3.0
      49.0       2.8
      50.0       5.3
      51.0       4.1
      52.0       3.8
      60.0       1.0
      61.0       4.2
      62.0       7.2
      62.5       2.1
      63.0       9.5
      64.0       2.3
      70.0       1.6
      71.0       1.1
      72.0       2.7
      73.0       9.2
      74.0      10.7
      75.0      16.6
      76.0       2.6
      77.0       5.5
      78.0       2.6
      83.0       1.6
      84.0       2.8
      85.0       3.5
      86.0       1.8
      87.0       1.9
      88.0       7.7
      89.0       5.2
      90.0       5.4
      97.0       5.6
      98.0       2.4
      99.0       4.1
     105.0       1.3
     107.0       1.8
     109.0       8.8
     110.0       2.5
     111.0      17.0
     112.0       3.7
     113.0       4.9
     114.0       2.5
     124.0      17.8
     125.0      18.3
     126.0       8.5
     127.0       6.2
     133.0      25.7
     134.0       2.3
     135.0      16.3
     136.0       1.2
     137.0       2.9
     141.0      16.0
     142.0       1.9
     143.0       5.0
     145.0       7.0
     146.0      11.1
     147.0       6.9
     148.0       7.6
     149.0       2.4
     150.0       1.7
     159.0      10.0
     160.0      59.5
     161.0      21.6
     162.0      39.3
     163.0      11.3
     164.0       7.1
     165.0       1.6
     174.0       2.4
     175.0       3.1
     176.0     100.0
     177.0       8.9
     178.0      62.0
     179.0       5.0
     180.0      10.2

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₆ Cl₂ N₂	0.039 g : 0.5 ml DMSO-d₆
(3,4-dichlorophenyl)hydrazine hydrochloride

    Assign.     Shift(ppm)

      A            10.6
      B             8.8
      C             7.517
      D             7.311
      E             7.021

     Hz     ppm     Int.

   4242.68  10.616    206
   3524.67   8.820     26
   3008.69   7.529    681
   3004.48   7.518     51
   2999.90   7.507    753
   2995.32   7.495     24
   2994.96   7.494     23
   2923.34   7.315    940
   2920.59   7.308   1000
   2811.61   7.036    541
   2808.86   7.029    518
   2806.11   7.022     55
   2805.56   7.021     54
   2802.81   7.014    511
   2800.07   7.007    503

in DMSO-d6

KBr disc

nujol mull

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