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MS-IW-4065 triethylene glycol monoisopropyl ether C9H20O4 (Mass of molecular ion: 192)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.8 18.0 1.1 19.0 3.5 27.0 9.3 28.0 8.8 29.0 5.3 30.0 1.2 31.0 9.0 33.0 1.9 39.0 1.9 41.0 12.6 42.0 4.7 43.0 78.9 44.0 29.1 45.0 100.0 46.0 5.3 47.0 1.1 55.0 3.0 57.0 7.2 58.0 33.5 59.0 21.3 60.0 3.5 61.0 3.5 62.0 1.8 63.0 3.2 69.0 3.6 71.0 1.1 72.0 15.3 73.0 23.7 74.0 1.2 75.0 51.7 76.0 7.2 86.0 32.2 87.0 22.7 88.0 14.2 89.0 47.9 90.0 6.8 101.0 1.8 103.0 4.2 104.0 1.6 106.0 2.3 107.0 1.3 117.0 3.2 119.0 7.0 133.0 4.5 134.0 1.1 151.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H20 O4 0.05 ml : 0.5 ml CDCl3 triethylene glycol monoisopropyl ether Assign. Shift(ppm)
A 3.72 B 3.67 C 3.64 D 3.60 E 1.168
Hz ppm Int.
1501.95 3.759 38 1491.82 3.733 167 1487.43 3.722 230 1482.67 3.710 211 1467.41 3.672 1000 1459.59 3.653 155 1455.81 3.643 245 1453.49 3.637 207 1450.44 3.630 285 1445.68 3.618 313 1440.55 3.605 278 1438.60 3.600 351 1435.06 3.591 241 1432.86 3.586 271 1428.96 3.576 135 1414.67 3.540 23 476.93 1.194 65 469.97 1.176 883 463.75 1.161 847
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