二环己烷并-18-冠醚-6

Mass

MS-NW-6514          
dicyclohexano-18-crown-6
C20H36O6            (Mass of molecular ion:    372)

   Source Temperature: 180 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      15.0       3.6
      19.0       2.2
      27.0       8.4
      28.0       7.9
      29.0       9.0
      31.0       8.6
      39.0       4.0
      40.0       1.0
      41.0      30.7
      42.0       8.4
      43.0      20.2
      44.0      14.1
      45.0     100.0
      46.0       2.3
      53.0       4.6
      54.0       5.8
      55.0      18.9
      56.0       2.1
      57.0      12.4
      58.0       5.7
      59.0       8.1
      64.0       1.3
      67.0      11.6
      68.0       2.8
      69.0      11.3
      70.0       8.3
      71.0       5.4
      72.0      17.0
      73.0      28.5
      74.0       1.2
      75.0       2.3
      77.0       1.1
      78.0       1.5
      79.0       7.1
      80.0       5.8
      81.0      59.9
      82.0      20.0
      83.0      15.2
      84.0       2.5
      85.0       1.7
      86.0       3.4
      87.0      15.8
      88.0      10.9
      89.0      36.0
      90.0       2.0
      91.0       1.3
      94.0       1.0
      95.0       2.3
      96.0       4.2
      97.0      13.5
      98.0      20.6
      99.0      41.2
     100.0       3.8
     101.0       4.8
     103.0       1.5
     105.0       1.7
     107.0       7.1
     108.0       1.1
     109.0       1.1
     111.0       1.2
     112.0       2.9
     113.0       3.4
     114.0       2.5
     115.0       2.0
     117.0       1.6
     119.0       1.4
     124.0       2.6
     125.0       2.3
     126.0       6.4
     127.0       7.6
     128.0       1.2
     129.0       1.8
     131.0       1.0
     133.0       1.7
     140.0       5.4
     141.0      12.8
     142.0       9.5
     143.0      23.9
     144.0       2.4
     155.0       4.3
     156.0       1.8
     157.0       1.5
     158.0       2.3
     159.0       1.1
     168.0       2.2
     169.0       2.2
     170.0       3.0
     171.0       2.8
     184.0       1.0
     185.0       6.8
     186.0       4.3
     187.0      10.8
     188.0       1.2
     203.0       1.0
     231.0       1.4

Assign. Shift(ppm) A 3.80 to 3.570 B 3.55 C 1.86 D 1.61 E 1.44 F 1.27

     Hz     ppm     Int.

   1467.90   3.673    426
   1466.43   3.670    315
   1463.01   3.661    519
   1458.62   3.650    245
   1457.15   3.647    209
   1453.86   3.638    231
   1452.03   3.634    147
   1449.95   3.629    238
   1447.51   3.622    131
   1445.56   3.618    119
   1444.46   3.615    127
   1432.25   3.584    107
   1431.76   3.583    106
   1424.07   3.564    122
   1423.71   3.563    124
   1423.10   3.561    128
   1421.75   3.558    131
   1420.90   3.556    130
   1420.41   3.555    131
   1420.04   3.554    133
   1419.68   3.553    134
   1419.07   3.551    133
   1417.36   3.547    119
   1413.33   3.537    123
   1412.96   3.536    122
   1411.25   3.532    125
    747.31   1.870    107
    746.58   1.869    104
    744.38   1.863    112
    743.65   1.861    114
    743.04   1.860    111
    742.19   1.858    107
    741.70   1.856    107
    739.26   1.850    117
    738.77   1.849    114
    736.45   1.843    105
    735.47   1.841    107
    735.11   1.840    108
    645.63   1.616    104
    644.90   1.614    106
    644.41   1.613    105
    643.19   1.610    104
    641.85   1.607    117
    641.24   1.605    119
    640.38   1.603    122
    639.16   1.600    114
    637.82   1.596    119
    636.11   1.592    127
    635.50   1.591    125
    635.01   1.589    120
    633.54   1.586    109
    633.18   1.585    110
    632.81   1.584    109
    632.57   1.583    109
    632.20   1.582    110
    631.35   1.580    112
    584.47   1.463    104
    582.03   1.457    111
    581.67   1.456    112
    575.07   1.439    107
    574.34   1.438    112
    573.85   1.436    112
    573.49   1.435    115
    572.75   1.434    116
    572.27   1.432    116
    571.78   1.431    115
    516.97   1.294    113
    514.04   1.287    137
    513.55   1.285    136
    513.31   1.285    136
    511.60   1.281    131
    508.79   1.274    158
    508.18   1.272    159
    505.37   1.265    148
    505.00   1.264    148
    504.52   1.263    146
    501.59   1.256    116
    500.49   1.253    120
    500.12   1.252    121
    499.63   1.251    122
    498.78   1.249    120