-
MS-NW-7111 allyltriethylammonium bromide C9H20BrN (Mass of molecular ion: 221)
Source Temperature: 230 °C Sample Temperature: 220 °C Direct, 75 eV
15.0 3.3 18.0 2.3 26.0 4.9 27.0 18.3 28.0 15.4 29.0 18.7 30.0 25.7 37.0 3.2 38.0 5.4 39.0 32.0 40.0 4.4 41.0 74.9 42.0 16.4 43.0 2.3 44.0 11.6 54.0 2.6 55.0 1.5 56.0 14.7 57.0 2.6 58.0 30.9 59.0 1.2 68.0 1.1 70.0 6.1 71.0 2.0 72.0 4.1 79.0 1.6 80.0 1.2 81.0 1.6 82.0 1.2 84.0 2.1 86.0 100.0 87.0 7.0 93.0 1.1 98.0 29.5 99.0 3.0 100.0 7.2 101.0 19.3 102.0 1.4 108.0 7.3 110.0 6.8 112.0 1.8 113.0 6.4 120.0 10.0 122.0 10.2
400 MHz in CDCl3
-
1H NMR 399.65 MHz C9 H20 Br N 0.041 g : 0.5 ml CDCl3 allyltriethylammonium bromide Assign. Shift(ppm)
A 5.992 B 5.831 C 5.720 D 4.112 E 3.488 F 1.428
Hz ppm Int.
2410.89 6.033 54 2408.08 6.026 33 2403.69 6.015 30 2401.00 6.008 92 2394.04 5.991 110 2391.24 5.984 51 2386.84 5.973 47 2384.03 5.966 103 2376.95 5.948 50 2337.28 5.849 169 2336.30 5.846 182 2320.56 5.807 104 2319.46 5.804 110 2291.26 5.734 164 2290.65 5.732 170 2290.28 5.731 169 2281.25 5.709 134 2280.64 5.707 141 2280.15 5.706 143 1647.09 4.122 315 1639.89 4.104 307 1405.03 3.516 322 1397.71 3.498 991 1390.38 3.479 1000 1383.06 3.461 336 578.00 1.447 509 570.80 1.429 947 563.48 1.410 485
更多供应商