图谱信息 供应商 相关产品
网站主页CAS数据库列表 29443-23-0更多图谱烯丙基三乙胺溴化物(29443-23-0)核磁图(1HNMR)

烯丙基三乙胺溴化物

产品名称 烯丙基三乙胺溴化物

CAS号29443-23-0

分子式C9H20BrN

分子量222.17

展开


  • Mass

    MS-NW-7111          
    allyltriethylammonium bromide
    C9H20BrN            (Mass of molecular ion:    221)
    

       Source Temperature: 230 °C
       Sample Temperature: 220 °C
       Direct, 75 eV
    

          15.0       3.3
          18.0       2.3
          26.0       4.9
          27.0      18.3
          28.0      15.4
          29.0      18.7
          30.0      25.7
          37.0       3.2
          38.0       5.4
          39.0      32.0
          40.0       4.4
          41.0      74.9
          42.0      16.4
          43.0       2.3
          44.0      11.6
          54.0       2.6
          55.0       1.5
          56.0      14.7
          57.0       2.6
          58.0      30.9
          59.0       1.2
          68.0       1.1
          70.0       6.1
          71.0       2.0
          72.0       4.1
          79.0       1.6
          80.0       1.2
          81.0       1.6
          82.0       1.2
          84.0       2.1
          86.0     100.0
          87.0       7.0
          93.0       1.1
          98.0      29.5
          99.0       3.0
         100.0       7.2
         101.0      19.3
         102.0       1.4
         108.0       7.3
         110.0       6.8
         112.0       1.8
         113.0       6.4
         120.0      10.0
         122.0      10.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H20 Br N 0.041 g : 0.5 ml CDCl3
    allyltriethylammonium bromide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.992 B 5.831 C 5.720 D 4.112 E 3.488 F 1.428

         Hz     ppm     Int.
    

       2410.89   6.033     54
       2408.08   6.026     33
       2403.69   6.015     30
       2401.00   6.008     92
       2394.04   5.991    110
       2391.24   5.984     51
       2386.84   5.973     47
       2384.03   5.966    103
       2376.95   5.948     50
       2337.28   5.849    169
       2336.30   5.846    182
       2320.56   5.807    104
       2319.46   5.804    110
       2291.26   5.734    164
       2290.65   5.732    170
       2290.28   5.731    169
       2281.25   5.709    134
       2280.64   5.707    141
       2280.15   5.706    143
       1647.09   4.122    315
       1639.89   4.104    307
       1405.03   3.516    322
       1397.71   3.498    991
       1390.38   3.479   1000
       1383.06   3.461    336
        578.00   1.447    509
        570.80   1.429    947
        563.48   1.410    485
    

in CDCl3



KBr disc



nujol mull