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网站主页CAS数据库列表 29440-91-3更多图谱4-甲基-Α-乙基-间酪胺(29440-91-3)核磁图(1HNMR)

4-甲基-Α-乙基-间酪胺

产品名称 4-甲基-Α-乙基-间酪胺

CAS号29440-91-3

分子式C11H18ClNO

分子量215.72

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400 MHz in DMSO-d6

90 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C11 H17 N O 0.019 g : 0.5 ml DMSO-d6
    5-(2-aminobutyl)-o-cresol hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.77 B 7.631 C 7.320 D 7.215 E 3.793 F *1 3.502 G *1 3.269 J 2.718 K 2.14 L 1.539 J(B,D)=7.8HZ. J(C,D)=1.4HZ. J(E,F)=5.5HZ. J(E,G)=8.5HZ. J(G,F)=-13.7HZ.

         Hz     ppm     Int.
    

       3505.49   8.772    171
       3053.83   7.642    158
       3046.02   7.622    173
       2926.03   7.322    222
       2924.68   7.319    241
       2888.06   7.227    130
       2886.60   7.223    126
       2880.37   7.208    120
       2879.03   7.204    118
       1523.19   3.812     45
       1522.71   3.811     46
       1521.24   3.807     40
       1520.75   3.806     41
       1520.02   3.804     42
       1518.19   3.799     48
       1516.60   3.795     61
       1515.50   3.793     58
       1515.01   3.791     60
       1511.96   3.784     41
       1511.35   3.782     42
       1510.38   3.780     41
       1509.40   3.777     46
       1508.54   3.775     51
       1409.55   3.527     62
       1404.05   3.514     60
       1395.87   3.493     79
       1390.38   3.479     69
       1316.65   3.295     82
       1307.98   3.273     83
       1305.05   3.266     32
       1302.86   3.261     70
       1294.56   3.240     63
       1086.30   2.719   1000
        875.00   2.190     30
        874.51   2.189     31
        867.68   2.172     69
        864.99   2.165     36
        862.30   2.158     69
        859.99   2.152     99
        856.69   2.144     45
        854.61   2.139     73
        851.93   2.132    108
        849.00   2.125     35
        848.14   2.123     34
        846.56   2.119     41
        844.73   2.114     84
        837.40   2.096     41
        622.31   1.558    285
        614.99   1.539    611
        607.42   1.520    256
    


  • 1H NMR 89.56 MHz
    C11 H17 N O 0.034 g : 0.5 ml DMSO-d6
    5-(2-aminobutyl)-o-cresol hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.3 B 8.2 C 6.979 D 6.719 E 6.580 F 3.15 G 3.07 to 2.51 J 2.084 K 1.52 L 0.915 DMSO SIGNAL AT 2.5 PPM REMOVED.

         Hz     ppm     Int.
    

        629.44   7.029    144
        622.00   6.946    214
        601.13   6.713    260
        593.06   6.622    163
        591.75   6.608    138
        585.63   6.539    109
        584.13   6.523    100
        282.06   3.150     79
        276.50   3.088     77
        271.19   3.029     91
        258.06   2.882    107
        253.06   2.826     83
        252.75   2.823     83
        245.38   2.740    110
        236.56   2.642     79
        186.63   2.084   1000
        143.69   1.605     92
        136.56   1.525    136
        136.19   1.521    136
        130.38   1.456    123
         88.06   0.984    261
         81.19   0.907    498
         73.38   0.820    140
    

in DMSO-d6



KBr disc