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MassMS-NW-7577 4-methylphenethylamine C9H13N (Mass of molecular ion: 135)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 2.5 27.0 2.0 28.0 2.4 30.0 100.0 31.0 1.5 39.0 3.4 41.0 1.0 50.0 1.2 51.0 3.2 52.0 1.2 53.0 1.6 63.0 1.9 65.0 2.8 77.0 7.1 78.0 2.5 79.0 4.2 89.0 1.1 91.0 15.9 92.0 1.4 103.0 3.5 104.0 2.8 105.0 13.3 106.0 39.5 107.0 3.7 115.0 1.2 117.0 2.1 118.0 2.7 119.0 1.3 132.0 1.5 135.0 6.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H13 N 0.05 ml : 0.5 ml CDCl3 4-methylphenethylamine 
Assign. Shift(ppm)
A 7.07 B 2.89 C 2.68 D 2.296 E 1.81
Hz ppm Int.633.13 7.070 1000 268.13 2.994 38 265.56 2.966 46 262.63 2.933 51 259.06 2.893 172 257.00 2.870 26 256.69 2.867 26 254.31 2.840 135 253.19 2.828 143 244.94 2.735 123 241.44 2.696 30 239.06 2.670 129 235.63 2.631 46 232.75 2.599 36 230.19 2.571 29 205.88 2.299 660 161.88 1.808 413
in CDCl3
liquid film
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