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MassMS-NW-7334 o-fluorophenylhydrazine hydrochloride C6H7FN2 HCl (Mass of molecular ion: 126)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 3.9 28.0 1.3 29.0 2.2 31.0 1.9 35.0 2.9 36.0 24.0 37.0 1.2 38.0 8.0 39.0 3.0 50.0 4.6 51.0 8.3 52.0 2.8 53.0 2.3 56.0 1.4 57.0 8.2 61.0 1.2 62.0 2.1 63.0 7.0 64.0 1.4 68.0 1.4 69.0 1.8 70.0 2.7 74.0 2.2 75.0 5.7 76.0 1.6 77.0 8.1 78.0 5.7 79.0 1.4 81.0 3.3 82.0 6.4 83.0 52.0 84.0 4.2 89.0 1.8 90.0 1.2 94.0 1.0 95.0 5.6 96.0 8.9 97.0 4.1 98.0 1.6 105.0 1.4 108.0 1.8 109.0 10.7 110.0 43.1 111.0 9.5 125.0 4.5 126.0 100.0 127.0 7.7 299.0 1.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H7 F N2 0.041 g : 0.5 ml DMSO-d6 o-fluorophenylhydrazine hydrochloride 
Assign. Shift(ppm)
A 10.5 B 8.33 C 7.279 D 7.197 E 7.144 G 6.979
Hz ppm Int.4199.82 10.509 850 3330.70 8.335 223 2918.94 7.304 400 2917.48 7.301 434 2909.42 7.280 841 2905.20 7.270 95 2902.09 7.262 590 2900.62 7.258 572 2887.44 7.225 509 2886.15 7.222 557 2879.38 7.205 626 2878.10 7.202 675 2875.53 7.196 542 2874.25 7.192 596 2867.47 7.175 616 2866.19 7.172 712 2863.08 7.164 554 2862.16 7.162 546 2855.57 7.146 1000 2854.83 7.144 931 2847.69 7.126 531 2846.59 7.123 502 2799.15 7.005 345 2797.69 7.001 362 2794.20 6.992 381 2792.74 6.988 450 2791.64 6.986 492 2791.09 6.984 489 2789.99 6.982 496 2786.70 6.973 501 2785.23 6.970 513 2783.76 6.966 343 2782.12 6.962 277 2778.64 6.953 261 2777.17 6.950 240
KBr disc
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