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网站主页CAS数据库列表 28069-72-9更多图谱反-2,顺6-壬二烯醇(28069-72-9)核磁图(13CNMR)

反-2,顺6-壬二烯醇

产品名称 反-2,顺6-壬二烯醇

CAS号28069-72-9

分子式C9H16O

分子量140.22

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  • Mass

    MS-IW-6968          
    trans,cis-2,6-nonadien-1-ol
    C9H16O              (Mass of molecular ion:    140)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          17.0       1.4
          18.0       7.4
          26.0       1.1
          27.0      24.4
          28.0       6.3
          29.0      16.1
          31.0       6.0
          38.0       1.4
          39.0      29.5
          40.0       5.3
          41.0     100.0
          42.0      13.8
          43.0      36.2
          44.0       2.4
          45.0       1.7
          50.0       2.1
          51.0       6.1
          52.0       3.2
          53.0      16.8
          54.0      37.4
          55.0      32.8
          56.0       4.2
          57.0      16.8
          58.0       1.7
          59.0       1.3
          63.0       1.9
          65.0       7.7
          66.0       8.5
          67.0      44.1
          68.0      64.9
          69.0      84.0
          70.0      26.9
          71.0       6.5
          72.0       1.6
          77.0      21.4
          78.0      12.4
          79.0      57.4
          80.0      22.3
          81.0      17.2
          82.0       5.5
          83.0       6.1
          84.0       2.1
          85.0       3.8
          91.0      20.4
          92.0       4.6
          93.0      48.9
          94.0      12.7
          95.0       4.2
          96.0       3.8
          97.0       6.7
          98.0       1.7
         105.0       3.3
         107.0      17.4
         108.0       1.9
         109.0      16.8
         110.0       1.7
         111.0       2.8
         120.0       1.0
         122.0      21.6
         123.0       2.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H16 O 0.05 ml : 0.5 ml CDCl3
    trans,cis-2,6-nonadien-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.67 B 5.65 C 5.38 D 5.32 E 4.063 F 2.65 G 2.107 J 2.031 K 0.954 ASSIGNED BY H-H COSY

         Hz     ppm     Int.
    

       2282.47   5.712     42
       2272.83   5.688     75
       2267.09   5.673    203
       2263.55   5.664    176
       2262.08   5.661    109
       2258.91   5.653    265
       2253.54   5.639    107
       2243.53   5.614     57
       2238.28   5.601     35
       2165.89   5.420     38
       2160.16   5.406     46
       2158.94   5.403     68
       2156.25   5.396     44
       2155.15   5.393     69
       2152.22   5.386     37
       2149.17   5.378     88
       2148.07   5.375    147
       2141.36   5.359     96
       2137.94   5.350     63
       2136.72   5.347     52
       2132.32   5.336     90
       2131.23   5.333    113
       2129.88   5.330     66
       2125.85   5.320     61
       2124.51   5.316     61
       2123.05   5.313     41
       2121.58   5.309     41
       2120.48   5.306     57
       2119.14   5.303     38
       1625.12   4.067    341
       1623.17   4.062    103
       1620.48   4.055    434
       1057.50   2.647     40
        857.91   2.147     43
        856.69   2.144     40
        851.44   2.131    124
        850.22   2.128    104
        846.19   2.118    219
        844.48   2.114    284
        842.29   2.108    387
        840.45   2.103    310
        838.99   2.100    229
        836.30   2.093     94
        835.21   2.090    109
        834.35   2.088    114
        833.50   2.086    118
        827.39   2.071     86
        823.97   2.062     41
        823.12   2.060     41
        819.95   2.052    169
        818.97   2.050    143
        812.62   2.034    238
        808.84   2.024     38
        805.66   2.016    159
        805.18   2.015    163
        804.57   2.014    150
        798.22   1.998     54
        797.61   1.996     48
        388.79   0.973    571
        381.23   0.954   1000
        373.66   0.935    564
    

in CDCl3



liquid film