反-2,顺6-壬二烯醇

Mass

MS-IW-6968          
trans,cis-2,6-nonadien-1-ol
C9H16O              (Mass of molecular ion:    140)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      17.0       1.4
      18.0       7.4
      26.0       1.1
      27.0      24.4
      28.0       6.3
      29.0      16.1
      31.0       6.0
      38.0       1.4
      39.0      29.5
      40.0       5.3
      41.0     100.0
      42.0      13.8
      43.0      36.2
      44.0       2.4
      45.0       1.7
      50.0       2.1
      51.0       6.1
      52.0       3.2
      53.0      16.8
      54.0      37.4
      55.0      32.8
      56.0       4.2
      57.0      16.8
      58.0       1.7
      59.0       1.3
      63.0       1.9
      65.0       7.7
      66.0       8.5
      67.0      44.1
      68.0      64.9
      69.0      84.0
      70.0      26.9
      71.0       6.5
      72.0       1.6
      77.0      21.4
      78.0      12.4
      79.0      57.4
      80.0      22.3
      81.0      17.2
      82.0       5.5
      83.0       6.1
      84.0       2.1
      85.0       3.8
      91.0      20.4
      92.0       4.6
      93.0      48.9
      94.0      12.7
      95.0       4.2
      96.0       3.8
      97.0       6.7
      98.0       1.7
     105.0       3.3
     107.0      17.4
     108.0       1.9
     109.0      16.8
     110.0       1.7
     111.0       2.8
     120.0       1.0
     122.0      21.6
     123.0       2.5

Assign. Shift(ppm) A 5.67 B 5.65 C 5.38 D 5.32 E 4.063 F 2.65 G 2.107 J 2.031 K 0.954 ASSIGNED BY H-H COSY

     Hz     ppm     Int.

   2282.47   5.712     42
   2272.83   5.688     75
   2267.09   5.673    203
   2263.55   5.664    176
   2262.08   5.661    109
   2258.91   5.653    265
   2253.54   5.639    107
   2243.53   5.614     57
   2238.28   5.601     35
   2165.89   5.420     38
   2160.16   5.406     46
   2158.94   5.403     68
   2156.25   5.396     44
   2155.15   5.393     69
   2152.22   5.386     37
   2149.17   5.378     88
   2148.07   5.375    147
   2141.36   5.359     96
   2137.94   5.350     63
   2136.72   5.347     52
   2132.32   5.336     90
   2131.23   5.333    113
   2129.88   5.330     66
   2125.85   5.320     61
   2124.51   5.316     61
   2123.05   5.313     41
   2121.58   5.309     41
   2120.48   5.306     57
   2119.14   5.303     38
   1625.12   4.067    341
   1623.17   4.062    103
   1620.48   4.055    434
   1057.50   2.647     40
    857.91   2.147     43
    856.69   2.144     40
    851.44   2.131    124
    850.22   2.128    104
    846.19   2.118    219
    844.48   2.114    284
    842.29   2.108    387
    840.45   2.103    310
    838.99   2.100    229
    836.30   2.093     94
    835.21   2.090    109
    834.35   2.088    114
    833.50   2.086    118
    827.39   2.071     86
    823.97   2.062     41
    823.12   2.060     41
    819.95   2.052    169
    818.97   2.050    143
    812.62   2.034    238
    808.84   2.024     38
    805.66   2.016    159
    805.18   2.015    163
    804.57   2.014    150
    798.22   1.998     54
    797.61   1.996     48
    388.79   0.973    571
    381.23   0.954   1000
    373.66   0.935    564