图谱信息 供应商 相关产品
网站主页CAS数据库列表 56805-23-3更多图谱3,6-亚壬基-1-醇(56805-23-3)质谱(MS)

3,6-亚壬基-1-醇

产品名称 3,6-亚壬基-1-醇

CAS号56805-23-3

分子式C9H16O

分子量140.22

展开


  • Mass

    MS-IW-6969          
    trans,cis-3,6-nonadien-1-ol
    C9H16O              (Mass of molecular ion:    140)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       4.0
          27.0      13.9
          28.0       4.2
          29.0      13.8
          31.0      10.5
          38.0       1.0
          39.0      21.6
          40.0       3.4
          41.0      44.0
          42.0       3.8
          43.0       9.9
          50.0       1.7
          51.0       5.1
          52.0       2.8
          53.0      14.4
          54.0      14.8
          55.0      42.8
          56.0       4.3
          57.0       4.9
          58.0       2.1
          63.0       1.6
          65.0       9.5
          66.0       5.5
          67.0     100.0
          68.0      30.4
          69.0       9.5
          70.0       6.8
          71.0       8.8
          72.0       3.8
          77.0      23.4
          78.0       5.2
          79.0      48.1
          80.0      14.9
          81.0      32.7
          82.0       4.8
          83.0       5.0
          84.0       8.4
          85.0       1.4
          86.0       1.0
          91.0      23.4
          92.0       3.9
          93.0      56.5
          94.0      10.5
          95.0      10.3
          96.0      13.0
          97.0       6.6
          98.0       9.6
         105.0       3.4
         107.0      16.3
         108.0       1.7
         109.0      18.2
         110.0       3.0
         111.0       4.2
         112.0       2.1
         122.0      17.3
         123.0       1.9
         140.0       6.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H16 O 0.05 ml : 0.5 ml CDCl3
    trans,cis-3,6-nonadien-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.52 B 5.44 C 5.42 D 5.34 E 3.607 F 2.759 G 2.37 J 2.260 K 2.044 L 0.962

         Hz     ppm     Int.
    

       2224.24   5.566     42
       2219.24   5.553     47
       2218.02   5.550     77
       2217.04   5.548     42
       2211.91   5.535     41
       2210.08   5.531     47
       2208.98   5.528     76
       2207.76   5.525     45
       2203.86   5.515     87
       2202.76   5.512    151
       2201.66   5.509     88
       2197.63   5.499     49
       2196.66   5.497     84
       2195.80   5.495     51
       2182.74   5.462     36
       2181.15   5.458     81
       2179.81   5.455     93
       2178.47   5.451     45
       2175.54   5.444     74
       2174.32   5.441    157
       2173.10   5.438    177
       2171.75   5.435    103
       2170.65   5.432     80
       2169.07   5.428     64
       2167.48   5.424     86
       2166.26   5.421    105
       2164.79   5.417    125
       2163.57   5.414    152
       2162.35   5.411     96
       2159.06   5.403     55
       2157.84   5.400    112
       2156.49   5.396    113
       2152.34   5.386     32
       2151.00   5.383     44
       2146.00   5.370     54
       2144.90   5.367     78
       2143.55   5.364     42
       2139.04   5.353     85
       2137.70   5.349    135
       2136.23   5.346     74
       2134.16   5.341     43
       2131.96   5.335     47
       2130.49   5.331     70
       2128.54   5.327     53
       2127.08   5.323     78
       2125.61   5.319     46
       2119.75   5.305     42
       1448.12   3.624    348
       1445.68   3.618     35
       1441.65   3.608    648
       1435.18   3.592    353
       1109.50   2.777    126
       1103.27   2.761    211
       1102.66   2.760    211
       1096.07   2.743    122
        947.27   2.371     66
        914.43   2.289     48
        913.33   2.286     94
        912.23   2.283     94
        911.25   2.281     55
        910.03   2.278     44
        907.84   2.272    123
        906.86   2.270    238
        905.64   2.267    237
        904.66   2.264    123
        901.25   2.256    126
        900.15   2.253    234
        899.05   2.250    231
        894.65   2.239     51
        893.55   2.236     89
        892.58   2.234     86
        833.13   2.085     41
        832.52   2.084     39
        831.79   2.082     39
        825.56   2.066    157
        824.83   2.064    141
        824.22   2.063    131
        817.99   2.047    231
        817.26   2.045    206
        810.91   2.030    162
        810.42   2.028    163
        809.69   2.026    146
        803.47   2.011     57
        802.86   2.009     55
        802.12   2.008     45
        391.97   0.981    578
        389.77   0.976     39
        384.52   0.963   1000
        376.95   0.944    548
    

in CDCl3



liquid film