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MS-IW-7440 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl acrylate C13H7F17O2 (Mass of molecular ion: 518)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.4 27.0 13.1 28.0 2.1 29.0 1.9 31.0 1.6 43.0 1.0 44.0 1.1 51.0 3.1 54.0 1.0 55.0 100.0 56.0 6.8 65.0 3.1 69.0 11.8 72.0 8.1 73.0 1.7 77.0 10.0 85.0 4.1 95.0 7.4 99.0 17.2 100.0 2.2 115.0 1.1 119.0 4.0 131.0 3.9 169.0 1.8 427.0 1.9 518.0 9.4 519.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H7 F17 O2 0.05 ml : 0.5 ml CDCl3 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl acrylate Assign. Shift(ppm)
A 6.442 B 6.132 C 5.874 D 4.473 E 2.521
Hz ppm Int.
2585.45 6.470 382 2583.98 6.466 380 2568.12 6.426 503 2566.65 6.423 509 2464.23 6.166 425 2453.74 6.140 530 2446.90 6.123 325 2436.40 6.097 400 2353.03 5.888 497 2351.68 5.885 473 2342.53 5.862 407 2341.19 5.859 407 1794.31 4.490 472 1787.72 4.474 1000 1781.25 4.458 511 1031.49 2.581 60 1025.02 2.565 114 1018.31 2.549 64 1013.31 2.536 122 1006.71 2.519 224 1000.24 2.503 115 995.00 2.490 72 988.40 2.474 122 981.93 2.457 60
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