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网站主页CAS数据库列表 27489-62-9更多图谱反式-4-氨基环己醇(27489-62-9)质谱(MS)

反式-4-氨基环己醇

产品名称 反式-4-氨基环己醇

CAS号27489-62-9

分子式C6H13NO

分子量115.17

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  • Mass

    MS-IW-9192          
    trans-4-aminocyclohexanol
    C6H13NO             (Mass of molecular ion:    115)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       3.4
          27.0       3.4
          28.0       6.5
          29.0       2.8
          30.0       5.7
          31.0       1.7
          39.0       2.9
          41.0       6.2
          42.0       5.5
          43.0      34.8
          44.0       2.3
          53.0       1.0
          54.0       2.0
          55.0       2.3
          56.0     100.0
          57.0      25.8
          58.0       1.4
          59.0       1.7
          68.0       5.5
          69.0       4.8
          77.0       1.0
          79.0       1.3
          81.0       1.0
          82.0       1.3
          96.0       1.6
          97.0       2.4
          98.0       1.3
         115.0       5.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H13 N O 0.039 g : 0.5 ml CDCl3
    trans-4-aminocyclohexanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.545 B 2.665 C 1.920 D 1.840 E 1.300 F 1.153

         Hz     ppm     Int.
    

       1431.52   3.582    272
       1427.25   3.572    519
       1423.10   3.561    322
       1420.90   3.556    534
       1416.63   3.545    977
       1412.35   3.534    531
       1410.28   3.529    309
       1406.01   3.519    490
       1401.61   3.508    249
       1080.44   2.704    256
       1076.42   2.694    494
       1072.39   2.684    307
       1069.46   2.676    543
       1065.55   2.667   1000
       1061.52   2.657    551
       1058.47   2.649    328
       1054.57   2.639    561
       1050.78   2.630    296
        776.00   1.942    738
        773.93   1.937    769
        772.83   1.934    765
        771.97   1.932    773
        768.31   1.923    578
        766.97   1.920    580
        763.31   1.910    809
        762.21   1.908    836
        761.23   1.905    853
        759.03   1.900    827
        755.74   1.892    412
        754.76   1.889    386
        751.95   1.882    183
        749.51   1.876    363
        748.41   1.873    393
        745.97   1.867    713
        744.87   1.864    757
        743.29   1.860    841
        742.55   1.859    826
        741.21   1.855    737
        739.87   1.852    674
        737.06   1.845    519
        735.96   1.842    529
        733.28   1.835    760
        731.81   1.832    798
        730.47   1.828    862
        728.27   1.823    724
        727.05   1.820    647
        542.97   1.359    359
        539.43   1.350    335
        529.66   1.326    859
        526.12   1.317    717
        518.55   1.298    771
        516.85   1.294    832
        516.24   1.292    824
        515.50   1.290    876
        513.55   1.285    573
        506.23   1.267    447
        502.93   1.259    467
        478.27   1.197    523
        475.10   1.189    495
        467.41   1.170    611
        465.33   1.165    968
        464.23   1.162    875
        462.16   1.157    748
        454.47   1.138    754
        452.15   1.132    702
        451.05   1.129    831
        441.28   1.105    295
        437.74   1.096    285
    

in CDCl3



KBr disc



nujol mull