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MassMS-IW-9192 trans-4-aminocyclohexanol C6H13NO (Mass of molecular ion: 115)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 3.4 27.0 3.4 28.0 6.5 29.0 2.8 30.0 5.7 31.0 1.7 39.0 2.9 41.0 6.2 42.0 5.5 43.0 34.8 44.0 2.3 53.0 1.0 54.0 2.0 55.0 2.3 56.0 100.0 57.0 25.8 58.0 1.4 59.0 1.7 68.0 5.5 69.0 4.8 77.0 1.0 79.0 1.3 81.0 1.0 82.0 1.3 96.0 1.6 97.0 2.4 98.0 1.3 115.0 5.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H13 N O 0.039 g : 0.5 ml CDCl3 trans-4-aminocyclohexanol 
Assign. Shift(ppm)
A 3.545 B 2.665 C 1.920 D 1.840 E 1.300 F 1.153
Hz ppm Int.1431.52 3.582 272 1427.25 3.572 519 1423.10 3.561 322 1420.90 3.556 534 1416.63 3.545 977 1412.35 3.534 531 1410.28 3.529 309 1406.01 3.519 490 1401.61 3.508 249 1080.44 2.704 256 1076.42 2.694 494 1072.39 2.684 307 1069.46 2.676 543 1065.55 2.667 1000 1061.52 2.657 551 1058.47 2.649 328 1054.57 2.639 561 1050.78 2.630 296 776.00 1.942 738 773.93 1.937 769 772.83 1.934 765 771.97 1.932 773 768.31 1.923 578 766.97 1.920 580 763.31 1.910 809 762.21 1.908 836 761.23 1.905 853 759.03 1.900 827 755.74 1.892 412 754.76 1.889 386 751.95 1.882 183 749.51 1.876 363 748.41 1.873 393 745.97 1.867 713 744.87 1.864 757 743.29 1.860 841 742.55 1.859 826 741.21 1.855 737 739.87 1.852 674 737.06 1.845 519 735.96 1.842 529 733.28 1.835 760 731.81 1.832 798 730.47 1.828 862 728.27 1.823 724 727.05 1.820 647 542.97 1.359 359 539.43 1.350 335 529.66 1.326 859 526.12 1.317 717 518.55 1.298 771 516.85 1.294 832 516.24 1.292 824 515.50 1.290 876 513.55 1.285 573 506.23 1.267 447 502.93 1.259 467 478.27 1.197 523 475.10 1.189 495 467.41 1.170 611 465.33 1.165 968 464.23 1.162 875 462.16 1.157 748 454.47 1.138 754 452.15 1.132 702 451.05 1.129 831 441.28 1.105 295 437.74 1.096 285
in CDCl3
KBr disc
nujol mull
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