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MassMS-KW-0199 2-methylnaphtho(1,2-d)thiazole C12H9NS (Mass of molecular ion: 199)
Source Temperature: 130 °C Sample Temperature: 110 °C Direct, 75 eV
45.0 1.2 63.0 1.7 66.0 1.5 69.0 1.6 77.5 1.2 79.0 13.2 79.5 1.6 87.0 1.0 88.0 1.3 93.0 1.0 99.5 9.0 100.0 1.5 113.0 3.7 114.0 10.1 115.0 3.3 127.0 1.2 153.0 2.6 154.0 3.9 157.0 1.1 158.0 14.9 159.0 4.5 160.0 1.1 166.0 2.7 167.0 3.8 171.0 1.6 198.0 17.2 199.0 100.0 200.0 15.1 201.0 5.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H9 N S 0.039 g : 0.5 ml CDCl3 2-methylnaphtho(1,2-d)thiazole 
Assign. Shift(ppm)
A 8.759 B 7.898 C 7.785 D 7.723 E *1 7.636 F *1 7.535 G 2.901
Hz ppm Int.3505.62 8.772 75 3504.88 8.770 79 3504.39 8.769 78 3497.31 8.751 78 3496.58 8.750 80 3496.09 8.748 80 3161.01 7.910 81 3152.83 7.889 88 3117.55 7.801 136 3108.76 7.779 250 3089.72 7.732 150 3080.93 7.710 81 3060.30 7.658 48 3059.08 7.655 49 3053.34 7.641 69 3052.12 7.637 101 3050.78 7.634 50 3045.17 7.620 64 3043.82 7.617 60 3018.80 7.554 72 3017.46 7.551 73 3011.84 7.537 59 3010.62 7.534 109 3009.40 7.531 68 3003.78 7.517 47 3002.44 7.513 46 1159.67 2.902 1000
in CDCl3
KBr disk
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