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MassMS-NW-7234 9-fluorenemethanol C14H12O (Mass of molecular ion: 196)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
31.0 1.6 39.0 1.5 51.0 1.1 62.0 1.2 63.0 3.0 69.5 2.3 74.0 1.3 75.0 1.5 76.0 1.7 81.5 1.9 82.0 1.7 82.5 2.9 86.0 1.1 87.0 1.7 88.0 2.1 89.0 1.8 115.0 3.2 139.0 4.7 152.0 1.5 162.0 1.3 163.0 11.0 164.0 9.4 165.0 100.0 166.0 79.8 167.0 11.3 176.0 1.7 177.0 1.4 178.0 7.5 179.0 1.5 196.0 33.6 197.0 5.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H12 O 0.036 g : 0.5 ml CDCl3 9-fluorenemethanol 
Assign. Shift(ppm)
A 7.745 B 7.566 C 7.372 D 7.292 E 4.056 F 3.967 J 1.75
Hz ppm Int.3099.24 7.755 842 3091.80 7.737 921 3027.71 7.576 757 3026.86 7.574 755 3020.14 7.557 861 3019.53 7.556 856 3013.31 7.540 30 2954.22 7.393 392 2946.90 7.374 859 2939.45 7.356 539 2935.67 7.346 58 2921.39 7.310 642 2920.29 7.308 655 2913.94 7.292 933 2912.84 7.289 917 2906.49 7.273 388 2905.40 7.270 367 1628.05 4.074 159 1621.95 4.059 368 1615.84 4.044 292 1588.26 3.975 1000 1582.15 3.959 707 700.93 1.754 362
in CDCl3
KBr disc
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