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MS-IW-1263 (2,2-dichlorocyclopropyl)benzene C9H8Cl2 (Mass of molecular ion: 186)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
38.0 1.2 39.0 5.0 50.0 3.7 51.0 6.4 52.0 1.2 57.0 6.9 57.5 6.7 58.0 2.2 61.0 1.2 62.0 3.0 63.0 7.8 64.0 1.5 65.0 3.5 73.0 1.8 74.0 2.9 74.5 1.1 75.0 5.0 75.5 1.0 76.0 1.9 77.0 4.0 78.0 3.0 86.0 1.1 87.0 1.6 88.0 1.0 89.0 9.0 90.0 2.5 91.0 4.0 102.0 1.3 103.0 2.7 104.0 2.1 113.0 1.4 114.0 2.6 115.0 100.0 116.0 21.7 117.0 1.6 125.0 2.1 149.0 5.3 150.0 3.1 151.0 64.5 152.0 7.2 153.0 20.4 154.0 2.0 186.0 18.4 187.0 2.1 188.0 11.8 189.0 1.2 190.0 1.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H8 Cl2 0.05 ml : 0.5 ml CDCl3 (2,2-dichlorocyclopropyl)benzene Assign. Shift(ppm)
A 7.314 B 7.273 C 7.214 D 2.868 E 1.910 F 1.810
Hz ppm Int.
2933.84 7.342 194 2932.13 7.337 335 2930.42 7.333 159 2927.37 7.325 218 2925.42 7.320 886 2923.58 7.316 576 2919.31 7.305 406 2917.85 7.302 1000 2912.84 7.289 257 2911.25 7.285 542 2909.67 7.281 385 2906.86 7.274 162 2904.17 7.267 553 2900.76 7.259 120 2898.32 7.253 99 2896.85 7.249 143 2895.51 7.246 75 2887.45 7.225 789 2885.86 7.221 970 2883.67 7.216 291 2879.27 7.205 702 2878.66 7.203 713 1156.25 2.894 331 1147.71 2.872 368 1145.63 2.867 385 1137.08 2.846 369 772.95 1.935 516 765.50 1.916 707 762.33 1.908 505 754.88 1.889 681 730.83 1.829 652 723.14 1.810 626 722.41 1.808 707 714.97 1.789 464
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