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MS-NW-7155 (1-naphthyl)hydrazine hydrochloride C10H10N2 HCl (Mass of molecular ion: 158)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
16.0 1.1 17.0 1.5 18.0 2.5 28.0 3.8 35.0 4.7 36.0 38.1 37.0 1.6 38.0 12.7 39.0 4.1 50.0 4.7 51.0 7.3 52.0 2.1 57.5 2.9 58.5 1.8 61.0 1.7 62.0 3.8 63.0 9.2 63.5 1.2 64.0 3.5 64.5 1.2 65.0 4.1 65.5 1.4 66.0 3.0 70.5 4.0 71.5 3.9 74.0 4.7 75.0 6.3 76.0 3.6 77.0 7.5 78.0 6.0 79.0 6.5 86.0 2.1 87.0 3.3 88.0 2.8 89.0 5.4 90.0 1.2 98.0 1.4 99.0 1.2 100.0 1.0 101.0 4.2 102.0 4.6 103.0 2.6 113.0 4.8 114.0 7.8 115.0 97.4 116.0 14.1 117.0 1.5 126.0 7.9 127.0 20.6 128.0 43.5 129.0 9.0 130.0 4.5 131.0 1.2 140.0 9.7 141.0 10.9 142.0 56.8 143.0 38.6 144.0 4.5 155.0 4.0 156.0 8.5 157.0 6.4 158.0 100.0 159.0 11.9 177.0 4.7 179.0 1.7
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H10 N2 0.035 g : 0.5 ml DMSO-d6 (1-naphthyl)hydrazine hydrochloride Assign. Shift(ppm)
A 10.5 B 8.9 C 8.062 D 7.904 E 7.54 F 7.448 G 7.020
Hz ppm Int.
4187.37 10.478 112 3575.41 8.947 38 3231.61 8.087 38 3226.66 8.074 312 3224.65 8.069 197 3223.73 8.067 191 3220.07 8.058 295 3216.77 8.049 334 3213.66 8.042 67 3213.11 8.040 72 3167.50 7.926 69 3167.13 7.925 69 3163.65 7.917 356 3160.35 7.908 349 3158.52 7.904 247 3156.33 7.898 243 3154.13 7.893 400 3151.38 7.886 66 3038.18 7.603 37 3036.90 7.599 37 3035.98 7.597 38 3035.44 7.596 37 3034.89 7.594 39 3034.52 7.593 40 3033.97 7.592 39 3033.24 7.590 43 3032.69 7.589 45 3032.14 7.587 48 3030.31 7.583 56 3029.76 7.582 55 3028.47 7.578 69 3028.11 7.577 69 3025.73 7.571 167 3024.45 7.568 151 3021.51 7.561 1000 3018.77 7.554 632 3017.67 7.551 890 3016.02 7.547 767 3014.55 7.543 560 3011.99 7.537 926 3008.88 7.529 777 3003.75 7.516 44 3003.38 7.516 42 3003.01 7.515 42 3002.65 7.514 42 3001.73 7.511 39 3001.37 7.510 40 2983.60 7.466 557 2980.12 7.457 65 2979.57 7.456 64 2976.09 7.447 721 2972.06 7.437 51 2971.51 7.436 43 2970.78 7.434 50 2968.03 7.427 409 2809.77 7.031 537 2809.04 7.029 560 2806.11 7.022 50 2802.45 7.013 516 2801.71 7.011 506
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