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MassMS-NW-6428 5,6,7,8-tetrahydro-1-naphthylamine C10H13N (Mass of molecular ion: 147)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.3 27.0 1.9 28.0 1.4 30.0 1.0 39.0 4.3 41.0 1.8 50.0 1.3 51.0 3.6 52.0 2.2 53.0 1.8 54.0 1.1 58.5 2.8 59.5 1.9 63.0 2.5 64.0 1.1 64.5 1.4 65.0 5.3 65.5 3.3 66.0 2.0 71.5 3.6 72.0 1.1 72.5 1.6 73.5 1.7 77.0 4.8 78.0 1.9 79.0 1.4 89.0 1.7 90.0 1.2 91.0 6.9 92.0 2.7 93.0 1.7 102.0 1.2 103.0 2.1 104.0 2.1 105.0 1.0 106.0 9.2 115.0 7.2 116.0 2.2 117.0 4.1 118.0 10.8 119.0 57.9 120.0 5.9 127.0 4.1 128.0 4.5 129.0 5.4 130.0 12.0 131.0 10.7 132.0 12.3 133.0 1.4 143.0 4.2 144.0 9.3 145.0 7.2 146.0 31.2 147.0 100.0 148.0 11.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H13 N 0.05 ml : 0.5 ml CDCl3 5,6,7,8-tetrahydro-1-naphthylamine 
Assign. Shift(ppm)
A 6.919 B 6.530 C 6.478 D 3.42 E 2.714 F 2.414 G *1 1.834 J *1 1.736
Hz ppm Int.2773.07 6.939 374 2765.38 6.920 758 2757.69 6.901 442 2613.04 6.539 550 2609.25 6.529 93 2605.47 6.520 521 2600.34 6.507 55 2599.73 6.506 54 2596.56 6.498 72 2596.19 6.497 72 2593.38 6.490 573 2592.77 6.488 591 2588.26 6.477 58 2585.57 6.470 512 2584.96 6.469 527 1366.09 3.419 345 1095.95 2.743 52 1090.82 2.730 505 1084.59 2.714 891 1078.61 2.699 535 971.07 2.430 490 964.84 2.415 1000 958.25 2.398 574 953.74 2.387 52 745.97 1.867 216 742.68 1.859 191 739.62 1.851 411 736.21 1.843 383 734.50 1.838 567 730.22 1.828 374 728.27 1.823 651 724.12 1.812 192 723.63 1.811 190 721.80 1.807 253 717.04 1.795 94 714.97 1.789 68 713.13 1.785 56 711.55 1.781 69 710.57 1.778 64 709.23 1.775 94 708.62 1.774 91 707.40 1.771 78 705.44 1.766 120 703.61 1.761 329 701.66 1.756 284 697.39 1.746 681 695.43 1.741 520 691.41 1.731 656 689.21 1.725 470 686.28 1.718 491 683.11 1.710 200 680.30 1.703 180 679.81 1.702 174
in CDCl3
liquid film
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