1-氨基四氢化萘

Mass

MS-NW-6428          
5,6,7,8-tetrahydro-1-naphthylamine
C10H13N             (Mass of molecular ion:    147)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.3
      27.0       1.9
      28.0       1.4
      30.0       1.0
      39.0       4.3
      41.0       1.8
      50.0       1.3
      51.0       3.6
      52.0       2.2
      53.0       1.8
      54.0       1.1
      58.5       2.8
      59.5       1.9
      63.0       2.5
      64.0       1.1
      64.5       1.4
      65.0       5.3
      65.5       3.3
      66.0       2.0
      71.5       3.6
      72.0       1.1
      72.5       1.6
      73.5       1.7
      77.0       4.8
      78.0       1.9
      79.0       1.4
      89.0       1.7
      90.0       1.2
      91.0       6.9
      92.0       2.7
      93.0       1.7
     102.0       1.2
     103.0       2.1
     104.0       2.1
     105.0       1.0
     106.0       9.2
     115.0       7.2
     116.0       2.2
     117.0       4.1
     118.0      10.8
     119.0      57.9
     120.0       5.9
     127.0       4.1
     128.0       4.5
     129.0       5.4
     130.0      12.0
     131.0      10.7
     132.0      12.3
     133.0       1.4
     143.0       4.2
     144.0       9.3
     145.0       7.2
     146.0      31.2
     147.0     100.0
     148.0      11.5

Assign. Shift(ppm) A 6.919 B 6.530 C 6.478 D 3.42 E 2.714 F 2.414 G *1 1.834 J *1 1.736

     Hz     ppm     Int.

   2773.07   6.939    374
   2765.38   6.920    758
   2757.69   6.901    442
   2613.04   6.539    550
   2609.25   6.529     93
   2605.47   6.520    521
   2600.34   6.507     55
   2599.73   6.506     54
   2596.56   6.498     72
   2596.19   6.497     72
   2593.38   6.490    573
   2592.77   6.488    591
   2588.26   6.477     58
   2585.57   6.470    512
   2584.96   6.469    527
   1366.09   3.419    345
   1095.95   2.743     52
   1090.82   2.730    505
   1084.59   2.714    891
   1078.61   2.699    535
    971.07   2.430    490
    964.84   2.415   1000
    958.25   2.398    574
    953.74   2.387     52
    745.97   1.867    216
    742.68   1.859    191
    739.62   1.851    411
    736.21   1.843    383
    734.50   1.838    567
    730.22   1.828    374
    728.27   1.823    651
    724.12   1.812    192
    723.63   1.811    190
    721.80   1.807    253
    717.04   1.795     94
    714.97   1.789     68
    713.13   1.785     56
    711.55   1.781     69
    710.57   1.778     64
    709.23   1.775     94
    708.62   1.774     91
    707.40   1.771     78
    705.44   1.766    120
    703.61   1.761    329
    701.66   1.756    284
    697.39   1.746    681
    695.43   1.741    520
    691.41   1.731    656
    689.21   1.725    470
    686.28   1.718    491
    683.11   1.710    200
    680.30   1.703    180
    679.81   1.702    174