[1S-(1α,2α,5β)]-5-甲基-2-(1-甲基乙基)环己醇

Mass

MS-IW-9205          
(1S-(1alpha,2alpha,5beta))-2-isopropyl-5-methylcyclohexanol
C10H20O             (Mass of molecular ion:    156)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       3.7
      27.0      12.7
      28.0       2.0
      29.0      13.1
      31.0       2.7
      39.0      11.9
      40.0       2.2
      41.0      38.9
      42.0       6.0
      43.0      28.9
      44.0       3.3
      45.0       2.1
      51.0       1.9
      52.0       1.0
      53.0       8.1
      54.0       4.6
      55.0      41.5
      56.0      18.3
      57.0      22.8
      58.0       2.9
      59.0       1.4
      65.0       2.0
      67.0      27.7
      68.0      15.8
      69.0      30.3
      70.0      11.0
      71.0     100.0
      72.0       5.6
      73.0       1.1
      77.0       3.0
      79.0       5.3
      80.0       5.4
      81.0      59.8
      82.0      30.7
      83.0      10.6
      84.0       2.9
      85.0       8.1
      86.0       3.8
      91.0       1.9
      93.0       3.2
      94.0       5.5
      95.0      77.1
      96.0      24.0
      97.0       4.1
      99.0       3.3
     109.0       8.9
     110.0       4.8
     111.0       1.5
     112.0       3.2
     113.0       1.8
     123.0      21.0
     124.0       2.1
     138.0      26.7
     139.0       3.8

Assign. Shift(ppm) A 4.103 B 1.835 C 1.74 to 1.71 D 1.66 E 1.53 F 1.50 G 1.277 J 1.083 K *1 0.957 L *1 0.917 M 0.869 N 0.86 ASSIGNED BY C-H COSY.

     Hz     ppm     Int.

   1641.24   4.107    165
   1638.79   4.101    162
    745.48   1.866     48
    742.07   1.857     95
    739.50   1.851    100
    735.96   1.842     54
    731.81   1.832     50
    728.39   1.823     99
    725.83   1.817    110
    722.29   1.808     58
    700.20   1.753     49
    696.90   1.744     98
    693.85   1.737    145
    690.92   1.729    132
    687.74   1.721     97
    683.47   1.711    115
    680.79   1.704    131
    677.61   1.696    141
    675.17   1.690    105
    674.32   1.688    109
    670.65   1.679     80
    666.38   1.668     41
    664.67   1.664     51
    663.82   1.662     51
    660.89   1.654     98
    657.35   1.645     90
    654.17   1.637     37
    622.80   1.559     79
    620.12   1.552     46
    616.09   1.542    113
    613.53   1.536     96
    609.50   1.526    104
    606.81   1.519    132
    602.78   1.509     76
    600.10   1.502    125
    596.19   1.492     57
    593.51   1.486     77
    528.69   1.323     42
    519.04   1.299    108
    515.87   1.291     90
    506.23   1.267    107
    502.93   1.259     96
    493.04   1.234     47
    489.62   1.226     42
    446.66   1.118     91
    444.09   1.112     87
    434.33   1.087    105
    432.50   1.083    134
    430.42   1.077     99
    420.78   1.053     78
    418.21   1.047     76
    406.62   1.018     42
    400.39   1.002     44
    385.74   0.966    978
    379.03   0.949    922
    369.87   0.926   1000
    363.28   0.909    939
    360.96   0.904    169
    356.57   0.893    174
    350.46   0.877    908
    344.12   0.862    929
    339.60   0.850    150
    336.55   0.843    107
    332.64   0.833     58
    330.08   0.826     45