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网站主页CAS数据库列表 2216-52-6更多图谱[1S-(1α,2α,5β)]-5-甲基-2-(1-甲基乙基)环己醇(2216-52-6)核磁图(1HNMR)

[1S-(1α,2α,5β)]-5-甲基-2-(1-甲基乙基)环己醇

产品名称 [1S-(1α,2α,5β)]-5-甲基-2-(1-甲基乙基)环己醇

CAS号2216-52-6

分子式C10H20O

分子量156.27

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  • Mass

    MS-IW-9205          
    (1S-(1alpha,2alpha,5beta))-2-isopropyl-5-methylcyclohexanol
    C10H20O             (Mass of molecular ion:    156)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       3.7
          27.0      12.7
          28.0       2.0
          29.0      13.1
          31.0       2.7
          39.0      11.9
          40.0       2.2
          41.0      38.9
          42.0       6.0
          43.0      28.9
          44.0       3.3
          45.0       2.1
          51.0       1.9
          52.0       1.0
          53.0       8.1
          54.0       4.6
          55.0      41.5
          56.0      18.3
          57.0      22.8
          58.0       2.9
          59.0       1.4
          65.0       2.0
          67.0      27.7
          68.0      15.8
          69.0      30.3
          70.0      11.0
          71.0     100.0
          72.0       5.6
          73.0       1.1
          77.0       3.0
          79.0       5.3
          80.0       5.4
          81.0      59.8
          82.0      30.7
          83.0      10.6
          84.0       2.9
          85.0       8.1
          86.0       3.8
          91.0       1.9
          93.0       3.2
          94.0       5.5
          95.0      77.1
          96.0      24.0
          97.0       4.1
          99.0       3.3
         109.0       8.9
         110.0       4.8
         111.0       1.5
         112.0       3.2
         113.0       1.8
         123.0      21.0
         124.0       2.1
         138.0      26.7
         139.0       3.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H20 O 0.05 ml : 0.5 ml CDCl3
    (1S-(1alpha,2alpha,5beta))-2-isopropyl-5-methylcyclohexanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.103 B 1.835 C 1.74 to 1.71 D 1.66 E 1.53 F 1.50 G 1.277 J 1.083 K *1 0.957 L *1 0.917 M 0.869 N 0.86 ASSIGNED BY C-H COSY.

         Hz     ppm     Int.
    

       1641.24   4.107    165
       1638.79   4.101    162
        745.48   1.866     48
        742.07   1.857     95
        739.50   1.851    100
        735.96   1.842     54
        731.81   1.832     50
        728.39   1.823     99
        725.83   1.817    110
        722.29   1.808     58
        700.20   1.753     49
        696.90   1.744     98
        693.85   1.737    145
        690.92   1.729    132
        687.74   1.721     97
        683.47   1.711    115
        680.79   1.704    131
        677.61   1.696    141
        675.17   1.690    105
        674.32   1.688    109
        670.65   1.679     80
        666.38   1.668     41
        664.67   1.664     51
        663.82   1.662     51
        660.89   1.654     98
        657.35   1.645     90
        654.17   1.637     37
        622.80   1.559     79
        620.12   1.552     46
        616.09   1.542    113
        613.53   1.536     96
        609.50   1.526    104
        606.81   1.519    132
        602.78   1.509     76
        600.10   1.502    125
        596.19   1.492     57
        593.51   1.486     77
        528.69   1.323     42
        519.04   1.299    108
        515.87   1.291     90
        506.23   1.267    107
        502.93   1.259     96
        493.04   1.234     47
        489.62   1.226     42
        446.66   1.118     91
        444.09   1.112     87
        434.33   1.087    105
        432.50   1.083    134
        430.42   1.077     99
        420.78   1.053     78
        418.21   1.047     76
        406.62   1.018     42
        400.39   1.002     44
        385.74   0.966    978
        379.03   0.949    922
        369.87   0.926   1000
        363.28   0.909    939
        360.96   0.904    169
        356.57   0.893    174
        350.46   0.877    908
        344.12   0.862    929
        339.60   0.850    150
        336.55   0.843    107
        332.64   0.833     58
        330.08   0.826     45
    

in CDCl3



liquid film