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MS-IW-5250 p-anisaldehyde dimethyl acetal C10H14O3 (Mass of molecular ion: 182)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.2 28.0 1.1 29.0 1.7 31.0 1.4 39.0 2.2 50.0 1.2 51.0 2.5 59.0 1.0 63.0 1.7 64.0 1.8 65.0 2.6 75.0 3.4 77.0 7.2 78.0 1.9 79.0 1.3 91.0 3.0 92.0 3.4 107.0 3.6 108.0 5.4 121.0 1.9 135.0 25.8 136.0 15.4 137.0 1.4 151.0 100.0 152.0 10.4 182.0 6.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H14 O3 0.05 ml : 0.5 ml CDCl3 p-anisaldehyde dimethyl acetal Assign. Shift(ppm)
A 7.361 B 6.883 C 5.341 D 3.779 E 3.298
Hz ppm Int.
2946.47 7.373 122 2944.79 7.369 43 2939.76 7.356 45 2938.08 7.352 140 2758.33 6.902 21 2755.43 6.895 159 2753.45 6.890 53 2748.72 6.878 50 2746.58 6.873 153 2135.01 5.343 150 1510.62 3.780 622 1318.21 3.299 1000
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