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MS-NW-6936 2,2'-dithiobis(5-nitropyridine) C10H6N4O4S2 (Mass of molecular ion: 310)
Source Temperature: 200 °C Sample Temperature: 120 °C Direct, 75 eV
17.0 1.4 18.0 6.3 28.0 1.4 29.0 1.3 30.0 7.0 37.0 1.2 38.0 5.6 39.0 3.7 40.0 4.0 44.0 1.1 45.0 5.8 46.0 5.8 50.0 5.7 51.0 4.8 52.0 3.5 57.0 2.0 58.0 1.1 64.0 5.4 65.0 2.2 69.0 4.5 70.0 4.2 71.0 1.3 76.0 2.2 77.0 7.7 78.0 1.6 80.0 1.2 81.0 4.0 82.0 14.9 83.0 5.5 84.0 1.2 96.0 2.1 97.0 1.2 98.0 2.3 108.0 1.8 109.0 4.1 110.0 3.7 112.0 2.1 123.0 19.2 124.0 1.7 141.0 6.5 142.0 1.4 154.0 6.5 155.0 1.8 156.0 7.2 157.0 1.2 158.0 1.3 170.0 14.9 171.0 2.0 185.0 1.4 186.0 1.2 187.0 10.7 188.0 1.1 189.0 1.2 191.0 1.5 200.0 11.0 201.0 1.6 217.0 1.3 218.0 3.8 220.0 1.0 231.0 4.4 232.0 1.7 246.0 1.0 264.0 2.9 277.0 6.1 278.0 2.9 310.0 100.0 311.0 14.5 312.0 11.2 313.0 1.5
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H6 N4 O4 S2 0.037 g : 0.5 ml DMSO-d6 2,2'-dithiobis(5-nitropyridine) Assign. Shift(ppm)
A 9.289 B 8.564 C 7.929
Hz ppm Int.
3714.29 9.294 942 3713.68 9.293 943 3711.55 9.288 1000 3710.94 9.286 889 3428.80 8.580 731 3426.21 8.574 681 3419.95 8.558 774 3417.21 8.551 754 3173.37 7.941 965 3172.76 7.939 895 3168.49 7.929 36 3164.52 7.919 900 3163.91 7.917 841
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