2,2'-二硫二吡啶

Mass

MS-IW-2318          
bis(2-pyridyl) disulfide
C10H8N2S2           (Mass of molecular ion:    220)

   Source Temperature: 100 °C
   Sample Temperature:  80 °C
   Direct, 75 eV

      27.0       2.1
      28.0       1.5
      38.0       1.8
      39.0      15.8
      40.0       1.1
      45.0       2.3
      50.0       3.5
      51.0      19.1
      52.0       6.7
      57.0       4.3
      58.0       1.4
      64.0       1.0
      66.0       1.5
      67.0       4.7
      69.0       2.7
      70.0       1.0
      76.0       1.1
      78.0      47.9
      79.0       5.8
      81.0       1.3
      82.0       3.9
      83.0       9.6
      84.0       3.2
     110.0       8.9
     111.0       5.1
     128.0       3.1
     129.0       9.6
     130.0       6.6
     142.0       2.6
     155.0      20.9
     156.0      62.5
     157.0       7.2
     187.0      16.1
     188.0       2.1
     219.0       1.4
     220.0     100.0
     221.0      13.5
     222.0       9.8
     223.0       1.2

Assign. Shift(ppm) A 8.462 B 7.64 C 7.59 D 7.112

     Hz     ppm     Int.

    761.69   8.505    190
    760.25   8.489    327
    758.88   8.474    211
    756.88   8.452    207
    755.69   8.438    302
    754.06   8.420    220
    689.38   7.698     34
    688.19   7.685     50
    685.06   7.650    700
    683.63   7.634   1000
    681.25   7.607    582
    680.19   7.595    930
    678.56   7.577    520
    672.13   7.505     53
    670.50   7.487     59
    647.31   7.228     56
    642.81   7.178    335
    638.94   7.135    299
    638.06   7.125    438
    634.44   7.084    387
    633.06   7.069    197
    629.50   7.029    219