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网站主页CAS数据库列表 2116-65-6更多图谱4-苄基吡啶(2116-65-6)核磁图(13CNMR)

4-苄基吡啶

产品名称 4-苄基吡啶

CAS号2116-65-6

分子式C12H11N

分子量169.22

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  • Mass

    MS-NW-0165          
    4-benzylpyridine
    C12H11N             (Mass of molecular ion:    169)
    

       Source Temperature: 220 °C
       Sample Temperature:  80 °C
       Reservoir, 75 eV
    

          27.0       1.5
          28.0       2.7
          38.0       1.4
          39.0       8.2
          41.0       1.3
          50.0       4.2
          51.0      10.9
          52.0       2.0
          54.0       2.3
          62.0       2.1
          63.0       6.7
          64.0       1.9
          65.0      10.1
          66.0       1.0
          70.5       1.0
          71.5       2.1
          74.0       1.4
          75.0       1.6
          76.0       1.3
          77.0       2.6
          78.0       1.3
          83.5       4.6
          87.0       1.1
          89.0       4.5
          90.0       1.8
          91.0      23.6
          92.0       2.4
         102.0       1.5
         113.0       1.0
         114.0       1.1
         115.0      10.8
         116.0       1.9
         127.0       1.0
         128.0       1.3
         139.0       5.7
         140.0       3.1
         141.0       8.3
         142.0       3.9
         154.0       2.4
         166.0       3.4
         167.0      22.1
         168.0      65.7
         169.0     100.0
         170.0      13.1
    

in DMSO-d6

400 MHz in CDCl3

90 MHz in CDCl3




  • 1H NMR 399.65 MHz
    C12 H11 N 34.7 mg : 0.5 ml CDCl3
    4-benzylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.489 B 7.308 C 7.244 D 7.171 E 7.093 F 3.954

         Hz     ppm     Int.
    

       3401.61   8.512     30
       3399.05   8.506     33
       3395.87   8.498    569
       3394.29   8.494    354
       3391.48   8.487    364
       3389.77   8.482    590
       2930.54   7.333    118
       2929.32   7.330    219
       2927.73   7.326    100
       2926.15   7.322     36
       2924.19   7.317    134
       2922.49   7.313    558
       2921.02   7.309    320
       2918.58   7.303     53
       2916.38   7.298    207
       2914.92   7.294    476
       2914.18   7.292    313
       2912.72   7.289    112
       2911.13   7.285     47
       2909.55   7.281     39
       2901.61   7.261    116
       2900.51   7.258    345
       2898.80   7.254    157
       2896.48   7.248     34
       2895.14   7.245     82
       2892.82   7.239    272
       2890.38   7.233     83
       2886.84   7.224     60
       2885.50   7.221     97
       2884.16   7.217     61
       2870.48   7.183    303
       2869.87   7.181    409
       2869.02   7.179    386
       2868.41   7.178    546
       2867.80   7.176    357
       2866.21   7.172    147
       2863.04   7.164    200
       2862.30   7.163    289
       2861.69   7.161    396
       2861.08   7.159    360
       2860.35   7.158    299
       2858.64   7.153     68
       2858.15   7.152     68
       2837.65   7.101    552
       2836.91   7.099    392
       2836.06   7.097    359
       2835.33   7.095    217
       2833.86   7.091    231
       2833.25   7.090    366
       2832.28   7.087    398
       2831.67   7.086    557
       2826.66   7.073     30
       1584.59   3.965     44
       1580.32   3.955   1000
    


  • 1H NMR 89.56 MHz
    C12 H11 N 0.035 g : 0.5 ml CDCl3
    4-benzylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.482 B 7.45 to 7.02 C 7.09 D 3.949

         Hz     ppm     Int.
    

        762.81   8.518    538
        761.19   8.500    335
        758.38   8.468    344
        756.75   8.450    601
        657.25   7.339    165
        656.81   7.334    133
        655.31   7.317    220
        654.13   7.304    118
        652.88   7.290    225
        651.81   7.278    619
        650.00   7.258    766
        649.44   7.252    884
        648.69   7.244    598
        645.13   7.204    661
        642.31   7.172    231
        641.19   7.160    228
        640.56   7.153    174
        639.81   7.144    164
        639.25   7.138    134
        637.31   7.117    679
        636.63   7.109    460
        635.69   7.098    400
        635.06   7.091    267
        633.63   7.075    221
        632.94   7.068    338
        632.00   7.057    360
        631.31   7.050    507
        353.69   3.950   1000
    

in CDCl3

in DMSO-d6





CCl4 solution



liquid film