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网站主页CAS数据库列表 101-82-6更多图谱2-苄基吡啶(101-82-6)核磁图(13CNMR)

2-苄基吡啶

产品名称 2-苄基吡啶

CAS号101-82-6

分子式C12H11N

分子量169.22

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  • Mass

    MS-NW-8485          
    2-benzylpyridine
    C12H11N             (Mass of molecular ion:    169)
    

       Source Temperature: 260 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          18.0       3.7
          27.0       2.1
          28.0       1.3
          39.0       5.5
          41.0       1.0
          50.0       3.6
          51.0      11.4
          52.0       2.9
          62.0       1.2
          63.0       3.7
          64.0       1.2
          65.0       6.6
          74.0       1.0
          75.0       1.1
          76.0       1.4
          77.0      13.5
          78.0       4.3
          83.5       4.8
          84.0       1.6
          89.0       2.7
          90.0       1.1
          91.0       5.9
         105.0       9.9
         115.0       2.7
         139.0       2.2
         140.0       1.5
         141.0       2.0
         154.0       3.5
         155.0      10.9
         156.0       1.3
         166.0       3.1
         167.0      21.8
         168.0     100.0
         169.0      23.9
         170.0       2.4
         182.0       4.8
         183.0       3.0
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H11 N 0.028 g : 0.5 ml CDCl3
    2-benzylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.54 B 7.535 C 7.35 to 7.18 D 7.09 E 4.153

         Hz     ppm     Int.
    

        768.50   8.581     60
        766.69   8.561     54
        765.94   8.553     74
        762.88   8.519     82
        761.75   8.506     62
        760.94   8.497     64
        677.31   7.563     65
        676.13   7.550     55
        675.25   7.540     66
        669.94   7.481     77
        668.06   7.460     81
        654.19   7.305     50
        652.63   7.288    115
        650.25   7.261   1000
        648.25   7.239    287
        646.31   7.217     86
        645.56   7.209     69
        643.88   7.190     45
        641.25   7.161     48
        640.19   7.149    108
        639.13   7.137    133
        637.63   7.120    133
        635.94   7.101    105
        634.50   7.085     47
        633.63   7.075     55
        633.19   7.071     45
        631.81   7.055     89
        630.88   7.045     75
        629.56   7.030     65
        629.13   7.025     64
        628.75   7.021     63
        627.44   7.006     45
        372.00   4.154    457
    


  • 1H NMR 399.65 MHz
    C12 H11 N 28.3 mg : 0.5 ml CDCl3
    2-benzylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.546 B 7.559 C 7.30 D 7.27 E 7.26 F 7.217 G 7.097 J 4.159 J(A,D)=5.6HZ. J(A,B)=1.8HZ.

         Hz     ppm     Int.
    

       3419.56   8.557    143
       3417.72   8.552    157
       3417.11   8.551    156
       3413.94   8.543    165
       3412.60   8.539    141
       3411.99   8.538    139
       3029.79   7.582    134
       3027.95   7.577    139
       3022.22   7.563    276
       3020.39   7.558    214
       3014.53   7.543    159
       3012.57   7.539    157
       2926.51   7.323     85
       2925.42   7.320    143
       2923.83   7.316     83
       2921.75   7.311     47
       2919.19   7.305    202
       2918.09   7.302    402
       2917.24   7.300    303
       2915.89   7.297     81
       2914.92   7.294     64
       2913.45   7.291    154
       2911.25   7.285    569
       2910.40   7.283    426
       2909.79   7.281    232
       2908.33   7.278    325
       2907.84   7.276    452
       2907.23   7.275    379
       2906.13   7.272    587
       2903.20   7.265    128
       2901.12   7.260    136
       2900.76   7.259    141
       2899.41   7.255    251
       2898.93   7.254    359
       2898.07   7.252    126
       2897.58   7.251    129
       2896.12   7.247     52
       2894.78   7.244     42
       2893.80   7.241     45
       2891.24   7.235    132
       2889.77   7.231    134
       2887.57   7.226     91
       2885.01   7.219     95
       2884.52   7.218     78
       2883.91   7.217     94
       2882.69   7.214    230
       2880.00   7.207     63
       2878.17   7.202     43
       2877.69   7.201     60
       2877.20   7.200     40
       2875.73   7.196     86
       2874.02   7.192     47
       2843.87   7.116     69
       2842.65   7.113    254
       2842.29   7.112    271
       2841.92   7.112    287
       2841.43   7.110    212
       2840.21   7.107    242
       2838.62   7.103    240
       2837.40   7.100    127
       2836.91   7.099    113
       2836.30   7.097    120
       2835.08   7.094    239
       2834.59   7.093    243
       2834.23   7.092    261
       2832.28   7.087    249
       2831.54   7.086    172
       2831.05   7.084    206
       2829.96   7.082    109
       1662.35   4.160   1000
    

in CDCl3



CCl4 solution



liquid film