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MassMS-KW-0523 5-chloro-2-fluoroaniline C6H5ClFN (Mass of molecular ion: 145)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 3.1 31.0 2.3 37.0 1.7 38.0 2.2 39.0 2.1 41.0 1.0 44.5 1.3 50.0 1.5 51.0 1.3 52.0 3.1 54.5 5.1 56.0 1.2 57.0 6.3 61.0 2.1 62.0 3.2 63.0 8.8 64.0 1.5 65.0 1.6 67.0 1.3 72.5 7.4 73.0 1.5 73.5 2.3 81.0 3.8 82.0 5.9 83.0 20.2 84.0 2.4 89.0 2.9 90.0 10.6 91.0 1.9 98.0 3.4 100.0 1.1 108.0 1.6 109.0 4.8 110.0 10.2 117.0 7.5 118.0 5.2 119.0 2.9 120.0 1.7 125.0 4.5 127.0 1.7 144.0 1.6 145.0 100.0 146.0 7.6 147.0 32.1 148.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C6H5ClFN 0.05 ml : 0.5 ml CDCl3 5-chloro-2-fluoroaniline 
Assign. Shift(ppm)
A 6.863 B 6.701 C 6.608 D 3.8
Hz ppm Int.2753.30 6.887 712 2744.63 6.866 853 2742.56 6.861 726 2733.89 6.839 812 2683.96 6.714 915 2681.52 6.708 1000 2676.15 6.695 896 2673.71 6.688 995 2648.93 6.626 706 2646.37 6.620 661 2644.90 6.616 734 2642.34 6.610 639 2640.26 6.605 619 2637.70 6.598 567 2636.24 6.595 619 2633.67 6.588 530 1551.52 3.881 26 1510.87 3.780 375
in CDCl3
Liquid film
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