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网站主页CAS数据库列表 2106-05-0更多图谱5-氯-2-氟苯胺(2106-05-0)核磁图(1HNMR)

5-氯-2-氟苯胺

产品名称 5-氯-2-氟苯胺

CAS号2106-05-0

分子式C6H5ClFN

分子量145.56

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  • Mass

    MS-KW-0523          
    5-chloro-2-fluoroaniline
    C6H5ClFN            (Mass of molecular ion:    145)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       3.1
          31.0       2.3
          37.0       1.7
          38.0       2.2
          39.0       2.1
          41.0       1.0
          44.5       1.3
          50.0       1.5
          51.0       1.3
          52.0       3.1
          54.5       5.1
          56.0       1.2
          57.0       6.3
          61.0       2.1
          62.0       3.2
          63.0       8.8
          64.0       1.5
          65.0       1.6
          67.0       1.3
          72.5       7.4
          73.0       1.5
          73.5       2.3
          81.0       3.8
          82.0       5.9
          83.0      20.2
          84.0       2.4
          89.0       2.9
          90.0      10.6
          91.0       1.9
          98.0       3.4
         100.0       1.1
         108.0       1.6
         109.0       4.8
         110.0      10.2
         117.0       7.5
         118.0       5.2
         119.0       2.9
         120.0       1.7
         125.0       4.5
         127.0       1.7
         144.0       1.6
         145.0     100.0
         146.0       7.6
         147.0      32.1
         148.0       2.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6H5ClFN 0.05 ml : 0.5 ml CDCl3
    5-chloro-2-fluoroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.863 B 6.701 C 6.608 D 3.8

         Hz     ppm     Int.
    

       2753.30   6.887    712
       2744.63   6.866    853
       2742.56   6.861    726
       2733.89   6.839    812
       2683.96   6.714    915
       2681.52   6.708   1000
       2676.15   6.695    896
       2673.71   6.688    995
       2648.93   6.626    706
       2646.37   6.620    661
       2644.90   6.616    734
       2642.34   6.610    639
       2640.26   6.605    619
       2637.70   6.598    567
       2636.24   6.595    619
       2633.67   6.588    530
       1551.52   3.881     26
       1510.87   3.780    375
    

in CDCl3



Liquid film