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MassMS-NW-9679 2-chloro-4-fluoroaniline C6H5ClFN (Mass of molecular ion: 145)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 1.5 31.0 1.2 52.0 2.1 54.5 3.7 56.0 1.1 57.0 4.2 61.0 1.1 62.0 1.9 63.0 3.8 72.5 5.2 73.5 1.6 81.0 3.4 82.0 13.8 83.0 18.0 84.0 1.9 89.0 2.7 90.0 3.7 91.0 1.2 108.0 2.4 109.0 10.9 110.0 10.8 117.0 5.9 118.0 5.3 119.0 2.3 120.0 1.7 144.0 2.2 145.0 100.0 146.0 7.7 147.0 32.4 148.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H5 Cl F N 0.05 ml : 0.5 ml CDCl3 2-chloro-4-fluoroaniline 
Assign. Shift(ppm)
A 6.991 B 6.781 C 6.647 D 3.9
Hz ppm Int.2799.80 7.006 900 2799.44 7.005 794 2796.88 6.999 912 2794.19 6.992 97 2793.82 6.991 101 2791.38 6.985 838 2788.57 6.978 946 2785.89 6.971 65 2785.52 6.970 66 2783.08 6.964 37 2722.90 6.814 37 2720.70 6.808 543 2717.77 6.801 559 2716.19 6.797 73 2712.65 6.788 675 2711.79 6.786 843 2709.72 6.781 653 2708.98 6.779 751 2706.05 6.772 81 2703.74 6.766 789 2700.93 6.759 722 2698.12 6.752 43 2663.33 6.665 958 2658.08 6.652 1000 2654.42 6.642 763 2652.10 6.637 82 2651.73 6.636 84 2649.29 6.630 723 2648.93 6.629 668 2642.82 6.613 31 1547.61 3.873 198
in CDCl3
liquid film
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