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MassMS-IW-4034 n-butylethylenediamine C6H16N2 (Mass of molecular ion: 116)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 5.8 27.0 4.2 28.0 6.5 29.0 16.5 30.0 65.2 31.0 1.3 39.0 2.4 41.0 17.4 42.0 7.6 43.0 6.1 44.0 72.4 45.0 2.2 55.0 3.2 56.0 7.1 57.0 16.3 58.0 2.0 70.0 2.7 71.0 2.4 72.0 2.3 73.0 7.1 83.0 1.6 84.0 2.4 85.0 2.2 86.0 100.0 87.0 6.7 98.0 1.3 99.0 2.1 116.0 5.0 117.0 1.2 127.0 5.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H16 N2 0.05 ml : 0.5 ml CDCl3 N-butylethylenediamine 
Assign. Shift(ppm)
A 2.801 B 2.672 C 2.604 D 2.08 E 1.477 F 1.351 G 0.919
Hz ppm Int.1125.73 2.817 106 1120.00 2.803 191 1114.14 2.788 140 1072.88 2.685 187 1066.89 2.670 208 1061.16 2.656 105 1048.22 2.623 160 1041.02 2.605 232 1033.69 2.587 168 830.57 2.079 273 606.57 1.518 60 605.83 1.516 57 599.61 1.501 144 596.68 1.494 84 592.41 1.483 169 591.55 1.481 193 590.94 1.479 194 589.23 1.475 98 584.11 1.462 178 581.91 1.457 108 577.15 1.445 103 576.54 1.443 101 557.50 1.395 59 550.54 1.378 161 542.60 1.358 201 541.87 1.356 176 534.79 1.339 210 527.71 1.321 132 520.75 1.304 50 374.27 0.937 567 366.94 0.919 1000 359.74 0.901 469
in CDCl3
liquid film
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