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MassMS-NW-1220 1-(2-aminoethyl)pyrrolidine C6H14N2 (Mass of molecular ion: 114)
Source Temperature: 250 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.7 18.0 2.7 27.0 3.5 28.0 6.8 29.0 3.0 30.0 10.3 39.0 2.0 41.0 4.2 42.0 29.8 43.0 4.6 44.0 4.1 54.0 1.3 55.0 13.7 56.0 4.4 57.0 1.4 70.0 3.9 82.0 1.1 84.0 100.0 85.0 6.3 114.0 3.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H14 N2 0.04 ml : 0.5 ml CDCl3 1-(2-aminoethyl)pyrrolidine 
Assign. Shift(ppm)
A 2.807 B 2.53 C 2.51 D 1.77 E 1.61
Hz ppm Int.260.13 2.905 218 258.38 2.885 253 254.50 2.842 295 252.94 2.825 382 252.19 2.816 895 247.31 2.762 580 246.25 2.750 665 236.06 2.636 39 234.69 2.621 47 232.69 2.599 660 231.69 2.587 673 230.63 2.576 260 230.00 2.569 254 229.19 2.560 211 228.19 2.548 256 227.75 2.543 273 226.81 2.533 1000 226.13 2.525 659 225.06 2.513 725 224.56 2.508 685 223.44 2.495 404 222.88 2.489 481 221.81 2.477 250 220.69 2.465 425 219.50 2.451 370 218.63 2.442 460 215.69 2.409 66 214.75 2.398 73 214.13 2.391 59 173.06 1.933 45 172.13 1.922 37 168.13 1.878 70 165.00 1.843 320 163.25 1.823 214 162.06 1.810 366 161.06 1.799 297 159.88 1.786 303 159.38 1.780 321 158.38 1.769 878 156.56 1.749 260 154.63 1.727 387 153.44 1.714 155 151.88 1.696 220 151.50 1.692 220 148.75 1.661 199 147.56 1.648 210 144.25 1.611 281 142.31 1.589 254
in CDCl3
CCl4 solution
liquid film
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