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MassMS-NW-2267 2-deoxy-D-galactose C6H12O5 (Mass of molecular ion: 164)
Source Temperature: 210 °C Sample Temperature: 170 °C Direct, 75 eV
13.0 2.2 14.0 7.7 15.0 30.9 16.0 1.4 17.0 10.7 18.0 52.9 19.0 22.3 25.0 2.1 26.0 9.4 27.0 36.8 28.0 31.4 29.0 92.8 30.0 14.3 31.0 100.0 32.0 26.8 33.0 1.3 37.0 2.3 38.0 3.6 39.0 24.0 40.0 6.5 41.0 19.8 42.0 26.3 43.0 94.0 44.0 75.9 45.0 57.0 46.0 5.9 47.0 4.9 51.0 1.6 53.0 5.5 54.0 3.9 55.0 23.8 56.0 38.2 57.0 75.4 58.0 20.1 59.0 2.4 60.0 50.6 61.0 34.4 62.0 2.7 68.0 14.7 69.0 13.7 70.0 5.2 71.0 22.4 72.0 11.8 73.0 28.2 74.0 37.5 75.0 6.9 81.0 6.2 82.0 3.2 83.0 2.0 84.0 4.2 85.0 29.3 86.0 36.4 87.0 4.4 91.0 2.8 97.0 11.6 98.0 5.1 99.0 4.3 100.0 1.9 102.0 2.4 103.0 34.0 104.0 1.7 110.0 3.0 111.0 1.4 115.0 9.0 116.0 1.3 117.0 1.5 128.0 4.4 129.0 1.2
400 MHz in D2O
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1H NMR 399.65 MHz C6 H12 O5 0.039 g : 0.5 ml D2O 2-deoxy-D-galactose 
Assign. Shift(ppm)
A 5.408 B 4.85 K 2.013 L 1.91 M 1.85 N 1.667 THE SOLVENT SIGNAL AT 4.8 PPM SUPPRESSED. PARTIALLY ASSIGNED.
Hz ppm Int.2162.23 5.411 288 2159.18 5.403 278 1943.24 4.863 117 1941.16 4.858 115 1639.53 4.103 122 1637.45 4.098 162 1634.28 4.090 207 1630.74 4.081 162 1627.69 4.073 138 1625.37 4.067 132 1622.07 4.059 233 1615.23 4.042 307 1609.13 4.027 170 1562.74 3.911 128 1559.45 3.903 161 1557.74 3.898 171 1554.57 3.890 163 1550.29 3.880 196 1547.36 3.872 481 1545.41 3.867 465 1514.53 3.790 133 1510.50 3.780 813 1507.45 3.772 464 1504.88 3.766 599 1503.05 3.761 671 1500.12 3.754 612 1493.65 3.738 1000 1487.43 3.722 830 1439.94 3.604 257 1439.21 3.602 237 1435.18 3.592 250 1434.20 3.589 257 1432.50 3.585 240 1431.52 3.582 206 1427.73 3.573 176 1426.64 3.570 161 812.01 2.032 119 809.45 2.026 121 808.84 2.024 112 807.25 2.020 122 802.12 2.008 127 801.27 2.005 129 799.93 2.002 142 797.24 1.995 141 796.63 1.994 130 795.04 1.990 135 769.90 1.927 175 766.11 1.917 169 757.81 1.897 192 754.15 1.888 168 746.83 1.869 225 741.58 1.856 201 682.62 1.709 145 672.73 1.684 133 670.41 1.678 277 660.64 1.654 220 658.33 1.648 153
KBr disc
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