400 MHz in D2O
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1H NMR 399.65 MHz C6 H12 O6 0.037 g : 0.5 ml D2O D-galactopyranose 
Assign. Shift(ppm)
A 5.268 B 4.587 C 4.091 D 3.987 E 3.929 F 3.853 G 3.82 J 3.78 to 3.72 K 3.648 L 3.494 MIXTURE OF ANOMERS. ASSIGNED BY H-H COSY. THE SOLVENT SIGNAL SUPPRESSED.
Hz ppm Int.2107.18 5.273 448 2103.52 5.264 477 1837.28 4.598 684 1829.35 4.578 710 1641.11 4.107 172 1635.50 4.093 295 1628.78 4.076 179 1595.34 3.992 333 1592.29 3.985 370 1572.14 3.934 421 1568.73 3.926 456 1549.19 3.877 180 1546.02 3.869 149 1538.82 3.851 431 1535.64 3.843 450 1527.59 3.823 473 1523.93 3.814 447 1520.63 3.805 114 1517.33 3.797 183 1513.55 3.788 230 1512.70 3.786 195 1509.03 3.776 370 1503.05 3.761 482 1501.22 3.757 851 1498.90 3.751 813 1495.73 3.743 1000 1490.48 3.730 545 1488.53 3.725 911 1484.50 3.715 300 1483.52 3.713 283 1480.71 3.706 214 1479.86 3.703 219 1476.68 3.695 189 1475.59 3.693 190 1465.58 3.668 315 1462.16 3.659 304 1455.69 3.643 421 1452.15 3.634 422 1404.91 3.516 386 1396.97 3.496 384 1395.02 3.491 349 1387.08 3.471 281
in D2O
KBr disc
nujol mull
4880 A,200 M,powder
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