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MassMS-NW-6413 2,2'-dithiodiethanol C4H10O2S2 (Mass of molecular ion: 154)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
14.0 2.5 15.0 10.9 17.0 3.0 18.0 13.3 19.0 12.7 26.0 4.6 27.0 25.3 28.0 4.9 29.0 17.9 30.0 1.3 31.0 38.6 32.0 1.5 34.0 1.3 35.0 1.0 42.0 3.9 43.0 23.8 44.0 10.4 45.0 100.0 46.0 18.4 47.0 24.1 48.0 7.9 49.0 11.1 57.0 1.1 58.0 4.1 59.0 14.1 60.0 21.4 61.0 20.2 62.0 1.7 63.0 1.2 64.0 51.9 65.0 2.6 66.0 6.1 74.0 1.2 75.0 3.3 76.0 10.4 77.0 4.1 78.0 6.6 79.0 43.7 80.0 3.4 81.0 4.6 82.0 7.6 89.0 4.2 91.0 3.8 92.0 90.4 93.0 5.3 94.0 8.3 107.0 6.1 108.0 2.6 109.0 1.4 110.0 12.2 112.0 1.3 123.0 1.2 136.0 1.7 154.0 49.2 155.0 3.3 156.0 4.9
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C4 H10 O2 S2 0.05 ml : 0.5 ml DMSO-d6 2,2'-dithiodiethanol 
Assign. Shift(ppm)
A 4.86 B 3.631 C 2.787
Hz ppm Int.1947.63 4.874 130 1942.63 4.861 306 1937.38 4.848 122 1460.21 3.654 169 1453.86 3.638 348 1448.61 3.625 334 1442.14 3.609 157 1120.12 2.803 618 1113.65 2.787 1000 1107.06 2.771 512 1101.56 2.757 21
in CDCl3
in DMSO-d6
liquid film
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