反式-4,5-二羟基-1,2-二噻烷

产品名称反式-4,5-二羟基-1,2-二噻烷

CAS号14193-38-5

分子式C4H8O2S2

分子量152.24

¹HNMR

¹³CNMR

IR1

IR2

Mass

MS-IW-0789          
trans-1,2-dithiane-4,5-diol
C4H8O2S2            (Mass of molecular ion:    152)

   Source Temperature: 130 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      15.0       1.8
      18.0       2.5
      19.0       1.2
      27.0       3.3
      28.0       1.8
      29.0       3.4
      31.0       3.3
      39.0       1.2
      41.0       2.3
      42.0       3.0
      43.0      19.9
      44.0      44.2
      45.0      18.9
      46.0      10.3
      47.0      13.3
      48.0       3.6
      55.0       7.0
      57.0       2.1
      58.0       1.8
      59.0       8.8
      60.0       7.7
      61.0       2.0
      63.0       1.3
      64.0      13.4
      66.0       2.0
      69.0       3.5
      70.0      25.6
      71.0       1.7
      73.0       2.6
      74.0       4.5
      75.0       2.0
      76.0       5.0
      77.0       8.4
      78.0       3.2
      79.0      16.5
      80.0       7.4
      81.0       1.7
      87.0      31.4
      88.0       2.2
      89.0       1.5
      91.0       2.0
      92.0       1.2
     101.0       8.1
     105.0       1.9
     108.0      66.7
     109.0       4.0
     110.0       6.2
     134.0      14.3
     135.0       1.8
     136.0       1.4
     152.0     100.0
     153.0       6.4
     154.0       9.4

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₄ H₈ O₂ S₂	0.035 g : 0.5 ml DMSO-d₆
trans-1,2-dithiane-4,5-diol

    Assign.     Shift(ppm)

      A             5.23
      B             3.344
      C     *1      3.041
      D     *1      2.739
     
     ASSIGNED BY C-H COSY

     Hz     ppm     Int.

   2097.78   5.250     39
   2091.19   5.233   1000
   2086.67   5.222    993
   2079.96   5.205     44
   1351.07   3.381     52
   1342.90   3.361    236
   1339.11   3.351    317
   1334.11   3.339    320
   1330.32   3.329    255
   1322.02   3.308     52
   1221.19   3.056    255
   1220.70   3.055    255
   1208.74   3.025    314
   1110.11   2.778     48
   1104.98   2.765    275
   1100.22   2.753    139
   1095.34   2.741    295
   1091.55   2.732    259
   1086.79   2.720    120
   1081.91   2.708    219
   1076.78   2.695     42

in DMSO-d6

KBr disc

nujol mull

更多供应商

反式-4,5-二羟基-1,2-二噻烷(14193-38-5)核磁图(¹HNMR) 相关产品图谱

反式-4,5-二羟基-1,2-二噻烷(14193-38-5)核磁图(¹³CNMR) 反式-4,5-二羟基-1,2-二噻烷(14193-38-5)质谱(MS) 反式-4,5-二羟基-1,2-二噻烷(14193-38-5)红外图谱(IR2) 反式-4,5-二羟基-1,2-二噻烷(14193-38-5)红外图谱(IR1) 反式-4,5-二羟基-1,2-二噻烷(14193-38-5)核磁图(¹HNMR)

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