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MS-IW-8153 (chloromethyl)dimethylphenylsilane C9H13ClSi (Mass of molecular ion: 184)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
43.0 4.4 51.0 1.1 53.0 2.3 63.0 2.8 65.0 2.2 67.5 1.6 77.0 1.0 79.0 2.3 91.0 9.0 93.0 4.4 95.0 1.4 105.0 4.7 107.0 4.0 119.0 2.4 133.0 2.8 135.0 100.0 136.0 14.1 137.0 4.2 141.0 4.0 143.0 1.5 153.0 1.6 155.0 1.1 169.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 Cl Si 0.05 ml : 0.5 ml CDCl3 (chloromethyl)dimethylphenylsilane Assign. Shift(ppm)
A 7.524 B 7.36 C 7.35 D 2.919 E 0.400
Hz ppm Int.
3012.45 7.538 134 3010.62 7.534 156 3009.40 7.531 56 3008.06 7.527 80 3007.32 7.525 71 3005.49 7.521 111 3003.91 7.517 82 3002.93 7.514 180 2948.24 7.378 43 2947.14 7.375 48 2946.66 7.374 54 2944.82 7.369 52 2943.73 7.366 152 2942.75 7.364 204 2941.65 7.361 209 2940.55 7.358 136 2939.09 7.355 107 2937.13 7.350 101 2936.40 7.348 106 2935.55 7.346 127 2935.06 7.345 127 2932.74 7.339 36 2931.64 7.336 32 2930.30 7.333 50 1166.63 2.920 547 163.33 0.409 158 160.16 0.401 1000 156.49 0.392 119
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