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MS-IW-9306 trimethylphenylsilane C9H14Si (Mass of molecular ion: 150)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 1.7 43.0 9.2 45.0 2.2 53.0 3.9 55.0 1.4 57.0 1.1 65.0 1.0 67.0 1.4 67.5 4.0 73.0 1.9 74.0 1.4 77.0 1.0 79.0 1.7 81.0 1.0 91.0 2.0 93.0 2.1 105.0 6.1 107.0 4.3 109.0 1.0 119.0 2.7 121.0 1.5 135.0 100.0 136.0 13.7 137.0 4.2 150.0 10.7 151.0 1.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H14 Si 0.05 ml : 0.5 ml CDCl3 trimethylphenylsilane Assign. Shift(ppm)
A 7.447 B 7.26 C 0.192
Hz ppm Int.
2982.42 7.463 35 2980.83 7.459 99 2979.25 7.455 71 2978.64 7.454 69 2977.29 7.450 122 2976.32 7.448 83 2973.75 7.441 117 2973.14 7.440 86 2971.31 7.435 112 2908.69 7.279 33 2907.35 7.275 64 2906.13 7.272 60 2904.54 7.268 161 2903.93 7.267 143 2902.83 7.264 169 2900.88 7.259 196 2898.07 7.252 220 80.32 0.201 229 76.90 0.193 1000 73.61 0.185 186
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