苯基乙烯基硫醚

Mass

MS-IW-3650          
phenyl vinyl sulfide
C8H8S               (Mass of molecular ion:    136)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      26.0       1.0
      27.0       3.6
      38.0       1.5
      39.0       7.4
      45.0       5.2
      50.0       5.7
      51.0      14.3
      52.0       1.5
      57.0       1.5
      58.0       5.4
      59.0       5.3
      62.0       1.1
      63.0       2.7
      65.0      11.5
      66.0       7.9
      67.0       4.2
      68.0       1.9
      69.0       6.6
      71.0       1.3
      74.0       2.3
      75.0       1.6
      76.0       1.2
      77.0      12.0
      78.0       3.1
      81.0       1.0
      82.0       2.0
      84.0       3.5
      89.0       1.1
      91.0      53.8
      92.0       5.0
     102.0       1.3
     103.0       3.7
     108.0       2.5
     109.0       9.2
     110.0       5.6
     121.0       4.6
     123.0       1.6
     134.0       8.2
     135.0     100.0
     136.0      89.1
     137.0      12.6
     138.0       4.4

Assign. Shift(ppm) A 7.357 B 7.283 C 7.216 D 6.512 E 5.321 F 5.318 J(D,E)=9.8 Hz J(D,F)=16.8 Hz J(E,F)=0.2 Hz

     Hz     ppm     Int.

   2947.39   7.375    128
   2946.47   7.373    375
   2945.10   7.370    584
   2942.96   7.364    210
   2939.91   7.357    230
   2939.00   7.354    322
   2938.08   7.352    599
   2937.47   7.351    519
   2936.71   7.349    693
   2934.57   7.343    148
   2920.68   7.309    133
   2919.92   7.307    270
   2918.85   7.304    520
   2916.87   7.299    228
   2913.82   7.291    143
   2913.21   7.290    152
   2912.45   7.288    477
   2911.68   7.286    920
   2910.16   7.282    458
   2907.26   7.275     46
   2905.58   7.271    281
   2903.90   7.267    393
   2903.44   7.265    455
   2901.76   7.261    119
   2900.85   7.259     56
   2891.08   7.235    280
   2889.71   7.231    497
   2888.34   7.228    277
   2886.35   7.223     35
   2884.67   7.218    178
   2882.08   7.212    364
   2879.94   7.207    125
   2878.11   7.202     38
   2876.43   7.198    102
   2875.21   7.195    193
   2873.84   7.191    114
   2616.12   6.547    445
   2606.51   6.522    502
   2599.33   6.505    490
   2589.87   6.481    502
   2133.94   5.340    961
   2131.35   5.334   1000
   2121.73   5.309    905
   2117.31   5.298    956
   2114.26   5.291     32