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网站主页CAS数据库列表 1822-73-7更多图谱苯基乙烯基硫醚(1822-73-7)核磁图(1HNMR)

苯基乙烯基硫醚

产品名称 苯基乙烯基硫醚

CAS号1822-73-7

分子式C8H8S

分子量136.21

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  • Mass

    MS-IW-3650          
    phenyl vinyl sulfide
    C8H8S               (Mass of molecular ion:    136)
    

       Source Temperature: 210 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          26.0       1.0
          27.0       3.6
          38.0       1.5
          39.0       7.4
          45.0       5.2
          50.0       5.7
          51.0      14.3
          52.0       1.5
          57.0       1.5
          58.0       5.4
          59.0       5.3
          62.0       1.1
          63.0       2.7
          65.0      11.5
          66.0       7.9
          67.0       4.2
          68.0       1.9
          69.0       6.6
          71.0       1.3
          74.0       2.3
          75.0       1.6
          76.0       1.2
          77.0      12.0
          78.0       3.1
          81.0       1.0
          82.0       2.0
          84.0       3.5
          89.0       1.1
          91.0      53.8
          92.0       5.0
         102.0       1.3
         103.0       3.7
         108.0       2.5
         109.0       9.2
         110.0       5.6
         121.0       4.6
         123.0       1.6
         134.0       8.2
         135.0     100.0
         136.0      89.1
         137.0      12.6
         138.0       4.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H8 S 0.05 ml : 0.5 ml CDCl3
    phenyl vinyl sulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.357 B 7.283 C 7.216 D 6.512 E 5.321 F 5.318 J(D,E)=9.8 Hz J(D,F)=16.8 Hz J(E,F)=0.2 Hz

         Hz     ppm     Int.
    

       2947.39   7.375    128
       2946.47   7.373    375
       2945.10   7.370    584
       2942.96   7.364    210
       2939.91   7.357    230
       2939.00   7.354    322
       2938.08   7.352    599
       2937.47   7.351    519
       2936.71   7.349    693
       2934.57   7.343    148
       2920.68   7.309    133
       2919.92   7.307    270
       2918.85   7.304    520
       2916.87   7.299    228
       2913.82   7.291    143
       2913.21   7.290    152
       2912.45   7.288    477
       2911.68   7.286    920
       2910.16   7.282    458
       2907.26   7.275     46
       2905.58   7.271    281
       2903.90   7.267    393
       2903.44   7.265    455
       2901.76   7.261    119
       2900.85   7.259     56
       2891.08   7.235    280
       2889.71   7.231    497
       2888.34   7.228    277
       2886.35   7.223     35
       2884.67   7.218    178
       2882.08   7.212    364
       2879.94   7.207    125
       2878.11   7.202     38
       2876.43   7.198    102
       2875.21   7.195    193
       2873.84   7.191    114
       2616.12   6.547    445
       2606.51   6.522    502
       2599.33   6.505    490
       2589.87   6.481    502
       2133.94   5.340    961
       2131.35   5.334   1000
       2121.73   5.309    905
       2117.31   5.298    956
       2114.26   5.291     32
    

in CDCl3



liquid film