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MassMS-NW-2164 5,5'-thiodisalicylic acid C14H10O6S (Mass of molecular ion: 306)
Source Temperature: 230 °C Sample Temperature: 250 °C Direct, 75 eV
12.0 2.3 16.0 4.3 17.0 3.8 18.0 13.8 26.0 1.4 27.0 4.6 28.0 11.5 29.0 2.4 37.0 2.3 38.0 6.7 39.0 24.4 40.0 1.9 43.0 1.5 44.0 71.0 45.0 17.7 47.0 1.1 50.0 4.6 51.0 7.0 52.0 2.1 53.0 15.1 54.0 1.1 55.0 4.2 58.0 1.0 61.0 2.7 62.0 8.7 63.0 26.8 64.0 7.3 65.0 11.1 66.0 3.9 67.0 1.9 69.0 15.2 70.0 9.6 71.0 4.6 72.0 1.4 74.0 2.1 75.0 2.2 76.0 1.1 77.0 3.0 78.0 1.3 79.0 8.4 79.5 1.4 80.0 1.6 81.0 8.2 82.0 1.8 85.0 4.7 85.5 1.2 86.0 1.6 87.0 1.0 89.0 3.4 90.0 1.3 91.0 3.5 92.0 5.6 93.0 3.4 93.5 2.1 94.0 12.5 94.5 1.0 95.0 23.5 96.0 5.3 97.0 9.3 98.0 4.6 99.0 1.0 100.0 1.5 101.0 1.0 102.0 1.9 107.0 2.4 108.0 2.8 109.0 1.5 114.0 2.9 115.0 14.5 116.0 3.1 117.0 1.0 118.0 3.4 119.0 1.3 120.0 2.9 121.0 1.9 122.0 6.8 123.0 2.6 124.0 2.8 125.0 8.8 126.0 5.5 127.0 4.3 128.0 4.0 129.0 1.3 131.0 6.3 132.0 1.3 133.0 1.2 134.0 1.7 135.0 2.8 137.0 4.5 138.0 1.3 139.0 1.0 143.0 1.4 144.0 6.8 145.0 2.2 147.0 1.1 150.0 1.1 151.0 4.1 152.0 1.8 155.0 11.4 156.0 2.6 157.0 6.6 158.0 11.3 159.0 5.6 160.0 3.0 161.0 1.9 162.0 1.7 163.0 2.8 169.0 1.2 170.0 1.5 171.0 13.2 172.0 2.1 173.0 1.6 176.0 4.5 183.0 2.6 184.0 2.8 185.0 5.1 186.0 10.0 187.0 37.4 188.0 57.3 189.0 11.8 190.0 3.7 191.0 2.3 199.0 3.7 200.0 2.6 201.0 2.6 202.0 1.2 203.0 1.2 214.0 9.5 215.0 5.0 216.0 5.9 217.0 7.9 218.0 35.7 219.0 5.6 220.0 2.4 243.0 5.0 244.0 100.0 245.0 15.5 246.0 6.8 261.0 1.8 262.0 75.1 263.0 11.2 264.0 5.2 270.0 14.1 271.0 3.0 272.0 1.1 288.0 12.4 289.0 2.4 290.0 1.0 306.0 10.6 307.0 1.7 308.0 1.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C14 H10 O6 S 0.040 g : 0.5 ml DMSO-d6 5,5'-thiodisalicylic acid 
Assign. Shift(ppm)
A 11. B 7.779 C 7.513 D 7.005
Hz ppm Int.3110.35 7.783 975 3107.97 7.777 1000 3104.31 7.768 27 3008.51 7.528 651 3005.95 7.522 643 2999.72 7.506 714 2997.34 7.500 729 2803.73 7.016 990 2799.70 7.006 31 2798.78 7.004 33 2795.12 6.994 935
in DMSO-d6
KBr disc
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