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MS-NW-8605 chlorodimethyloctylsilane C10H23ClSi (Mass of molecular ion: 206)
Source Temperature: 250 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 2.0 29.0 2.9 39.0 1.5 41.0 5.1 42.0 1.4 43.0 5.1 55.0 2.4 56.0 1.5 57.0 5.3 59.0 3.2 63.0 2.9 65.0 4.6 67.0 1.3 69.0 2.7 70.0 1.8 71.0 1.4 73.0 1.0 78.0 1.4 79.0 8.7 80.0 1.0 81.0 3.1 83.0 1.5 84.0 1.0 91.0 1.3 92.0 1.7 93.0 100.0 94.0 7.9 95.0 36.0 96.0 2.5 97.0 2.1 105.0 1.5 107.0 5.0 109.0 1.6 111.0 3.7 112.0 4.9 119.0 4.9 121.0 15.9 122.0 1.5 123.0 5.4 133.0 12.2 134.0 1.8 135.0 3.6 137.0 1.1 147.0 3.5 149.0 2.3 191.0 18.7 192.0 2.8 193.0 6.8 194.0 1.0 245.0 2.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H23 Cl Si 0.05 ml : 0.5 ml CDCl3 chlorodimethyloctylsilane Assign. Shift(ppm)
A 1.30 B 1.27 C 0.883 D 0.499 E 0.028
Hz ppm Int.
529.05 1.324 60 519.41 1.300 160 516.85 1.294 166 514.28 1.287 192 506.96 1.269 353 359.86 0.901 102 353.15 0.884 296 346.07 0.866 124 207.03 0.519 42 199.22 0.499 66 191.53 0.480 43 14.65 0.037 99 11.35 0.029 1000 8.06 0.021 105 3.30 0.009 21
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